4-((1S,2S)-1-hydroxy-1-(4-hydroxy-3-methoxyphenyl)propan-2-yloxy)-3-methoxybenzaldehyde

Base Information

Chemical Name:4-((1S,2S)-1-hydroxy-1-(4-hydroxy-3-methoxyphenyl)propan-2-yloxy)-3-methoxybenzaldehyde
CAS No.:186033-12-5
Molecular Formula:C₁₈H₂₀O₆
Molecular Weight:332.353
Hs Code.:

Synonyms:4-((1S,2S)-1-hydroxy-1-(4-hydroxy-3-methoxyphenyl)propan-2-yloxy)-3-methoxybenzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-((1S,2S)-1-hydroxy-1-(4-hydroxy-3-methoxyphenyl)propan-2-yloxy)-3-methoxybenzaldehyde

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Technology Process of 4-((1S,2S)-1-hydroxy-1-(4-hydroxy-3-methoxyphenyl)propan-2-yloxy)-3-methoxybenzaldehyde

There total 1 articles about 4-((1S,2S)-1-hydroxy-1-(4-hydroxy-3-methoxyphenyl)propan-2-yloxy)-3-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1240326-76-4
(1S,2S)-1-(4-(benzyloxy)-3-methoxyphenyl)-1-(tetrahydro-2H-pyran-2-yloxy)propan-2-ol

: 121-33-5,8014-42-4
vanillin

: 186033-12-5
4-((1S,2S)-1-hydroxy-1-(4-hydroxy-3-methoxyphenyl)propan-2-yloxy)-3-methoxybenzaldehyde

Guidance literature:: (1S,2S)-1-(4-(benzyloxy)-3-methoxyphenyl)-1-(tetrahydro-2H-pyran-2-yloxy)propan-2-ol; vanillin; With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 24h; Reflux; Inert atmosphere;

With hydrogenchloride; In methanol; at 20 ℃; for 8h; Inert atmosphere;

With palladium 10% on activated carbon; hydrogen; In methanol; ethyl acetate; at 20 ℃; for 8h; under 760.051 Torr; optical yield given as %de;
DOI:10.3906/kim-0908-201