anti-(2RS,3RS)-1,3-Diphenyl-2-methyl-3-<(trimethylsilyl)oxy>propan-1-one

Base Information

Chemical Name:anti-(2RS,3RS)-1,3-Diphenyl-2-methyl-3-<(trimethylsilyl)oxy>propan-1-one
CAS No.:133225-48-6
Molecular Formula:C₁₉H₂₄O₂Si
Molecular Weight:312.484
Hs Code.:

Synonyms:anti-(2RS,3RS)-1,3-Diphenyl-2-methyl-3-<(trimethylsilyl)oxy>propan-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of anti-(2RS,3RS)-1,3-Diphenyl-2-methyl-3-<(trimethylsilyl)oxy>propan-1-one

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Technology Process of anti-(2RS,3RS)-1,3-Diphenyl-2-methyl-3-<(trimethylsilyl)oxy>propan-1-one

There total 14 articles about anti-(2RS,3RS)-1,3-Diphenyl-2-methyl-3-<(trimethylsilyl)oxy>propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 37471-46-8
1-phenyl-1-trimethylsiloxypropene

: 100-52-7
benzaldehyde

: 133225-48-6
anti-(2RS,3RS)-1,3-Diphenyl-2-methyl-3-<(trimethylsilyl)oxy>propan-1-one

Guidance literature:: bis(triphenyl)oxodiphosphonium trifluoromethanesulfonate salt; In dichloromethane; at -78 ℃;

Reference yield: 90.0%

: 66323-99-7
trimethyl[(Z)-(1-phenyl-1-propenyl)oxy]silane

: 100-52-7
benzaldehyde

: 133225-48-6
anti-(2RS,3RS)-1,3-Diphenyl-2-methyl-3-<(trimethylsilyl)oxy>propan-1-one

Guidance literature:: With trimethylsilyl bis(trifluoromethanesulfonyl)imide; In diethyl ether; at -78 ℃;
DOI:10.1039/b203838b

Reference yield:

: 66323-99-7
trimethyl[(Z)-(1-phenyl-1-propenyl)oxy]silane

: 104-55-2
3-phenyl-propenal

: 133225-48-6
anti-(2RS,3RS)-1,3-Diphenyl-2-methyl-3-<(trimethylsilyl)oxy>propan-1-one

Guidance literature:: With borane-THF; (2R,3R)-3-hydroxy-2-<(2,6-diisopropoxybenzoyl)oxy>butanedioic acid; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1021/ja00003a047