Ile-Ser(Dpp)-Leu

Base Information

Chemical Name:Ile-Ser(Dpp)-Leu
CAS No.:75816-58-9
Molecular Formula:BrH*C₂₇H₃₈N₃O₈P
Molecular Weight:644.5
Hs Code.:

Synonyms:Ile-Ser(Dpp)-Leu

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ile-Ser(Dpp)-Leu

Chemical Property:

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Technology Process of Ile-Ser(Dpp)-Leu

There total 7 articles about Ile-Ser(Dpp)-Leu which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 75816-64-7
Z-Ile-Ser(Dpp)-Leu-OBu^t

: 75816-58-9
Ile-Ser(Dpp)-Leu

Guidance literature:: With hydrogen bromide; In acetic acid; for 0.75h;

Reference yield:

: 28252-48-4
Z-Ser-Leu-OBu^t

: 75816-58-9
Ile-Ser(Dpp)-Leu

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) hydrogen, 2.) 0.4N-hydrogen chloride / 1.) 10percent palladium-charcoal / 1.) 1percent acetic acid in methanol, 2.5 h, 2.) methanol, -15 deg C

2: 90 percent / triethylamine / tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) room temperature, 1 h

3: 76 percent / pyridine / 4 h / 0 °C

4: 97 percent / 2N hydrogen bromide / acetic acid / 0.75 h

With hydrogenchloride; hydrogen bromide; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; acetic acid;

Reference yield:

: 3160-59-6
N-Cbz-L-Isoleucine

: 75816-58-9
Ile-Ser(Dpp)-Leu

Guidance literature:: Multi-step reaction with 4 steps

1: N-methylmorpholine / tetrahydrofuran / 0.17 h / -15 °C

2: 90 percent / triethylamine / tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) room temperature, 1 h

3: 76 percent / pyridine / 4 h / 0 °C

4: 97 percent / 2N hydrogen bromide / acetic acid / 0.75 h

With 4-methyl-morpholine; hydrogen bromide; triethylamine; In tetrahydrofuran; pyridine; acetic acid;