1-(2,5-Dimethoxy-2,5-dihydrofuran-2-yl)ethan-1-ol

Base Information

Chemical Name:1-(2,5-Dimethoxy-2,5-dihydrofuran-2-yl)ethan-1-ol
CAS No.:33647-67-5
Molecular Formula:C8H14 O4
Molecular Weight:174.197
Hs Code.:2932190090
DSSTox Substance ID:DTXSID90955272
Wikidata:Q82934792
Mol file:33647-67-5.mol

Synonyms:DTXSID90955272;1-(2,5-Dimethoxy-2,5-dihydrofuran-2-yl)ethan-1-ol

Suppliers and Price of 1-(2,5-Dimethoxy-2,5-dihydrofuran-2-yl)ethan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
DL-1-(2,5-DIMETHOXY-2,5-DIHYDROFURAN-2-YL)ETHANOL 95.00%
5MG
$ 497.16

Total 8 raw suppliers

Chemical Property of 1-(2,5-Dimethoxy-2,5-dihydrofuran-2-yl)ethan-1-ol

Chemical Property:

Vapor Pressure:0.00171mmHg at 25°C
Refractive Index:1.4455 (estimate)
Boiling Point:64-68 °C (1 mmHg)
Flash Point:111.6°C
PSA：47.92000
Density:1.13g/cm³
LogP:0.26880
Storage Temp.:0-6°C
XLogP3:-0.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:174.08920892
Heavy Atom Count:12
Complexity:180

Purity/Quality:

99% ^*data from raw suppliers

DL-1-(2,5-DIMETHOXY-2,5-DIHYDROFURAN-2-YL)ETHANOL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 24/25

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C1(C=CC(O1)OC)OC)O
Isomeric SMILES:C[C@@H]([C@@]1(C=C[C@@H](O1)OC)OC)O

Technology Process of 1-(2,5-Dimethoxy-2,5-dihydrofuran-2-yl)ethan-1-ol

There total 9 articles about 1-(2,5-Dimethoxy-2,5-dihydrofuran-2-yl)ethan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 4208-64-4
1-(2-furyl)ethanol

: 67-56-1
methanol

: 33647-67-5,316186-17-1,236408-20-1
1-(2,5-dimethoxy-2,5-dihydrofuran-2-yl)ethanol from 2-Acetylfuran

Guidance literature:: With piperidine; silica gel; Electrochemical reaction;
DOI:10.1002/chem.200500340

Reference yield: 89.0%

: 67-56-1
methanol

: 4208-64-4,27948-61-4,106565-48-4,112653-32-4
(S)-1-(2-furanyl)ethanol

: 33647-67-5,316186-17-1,236408-20-1
(S)-1-(2,5-dihydro-2,5-dimethoxy-2-furyl)ethanol

Guidance literature:: With bromine; In diethyl ether; at -40 ℃; for 0.5h;
DOI:10.1016/j.carres.2006.01.019

Reference yield:

: 1192-62-7,80145-44-4
1-(2-furyl)-1-ethanone

: 33647-67-5,316186-17-1,236408-20-1
(S)-1-(2,5-dihydro-2,5-dimethoxy-2-furyl)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Et₃N / Ru(II) complex from (1S,2S)-N-(pTs)-1,2-diPhethylenediamine / formic acid / 42 h / 20 °C

2: 89 percent / Br₂ / diethyl ether / 0.5 h / -40 °C

With bromine; triethylamine; Ru(II)-(1S,2S)-N-p-toluenesulfonyl-1,2-di-Ph-ethylenediamine; In formic acid; diethyl ether;
DOI:10.1016/j.carres.2006.01.019