(7S)-7-deoxy-7-[5-(5-dimethylamino-4-fluoro-2-nitrophenyl)-1,3,4-thiadiazol-2-ylthio]lincomycin

Base Information

Chemical Name:(7S)-7-deoxy-7-[5-(5-dimethylamino-4-fluoro-2-nitrophenyl)-1,3,4-thiadiazol-2-ylthio]lincomycin
CAS No.:941586-78-3
Molecular Formula:C₂₈H₄₁FN₆O₇S₃
Molecular Weight:688.866
Hs Code.:

Synonyms:(7S)-7-deoxy-7-[5-(5-dimethylamino-4-fluoro-2-nitrophenyl)-1,3,4-thiadiazol-2-ylthio]lincomycin

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Chemical Property of (7S)-7-deoxy-7-[5-(5-dimethylamino-4-fluoro-2-nitrophenyl)-1,3,4-thiadiazol-2-ylthio]lincomycin

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Technology Process of (7S)-7-deoxy-7-[5-(5-dimethylamino-4-fluoro-2-nitrophenyl)-1,3,4-thiadiazol-2-ylthio]lincomycin

There total 5 articles about (7S)-7-deoxy-7-[5-(5-dimethylamino-4-fluoro-2-nitrophenyl)-1,3,4-thiadiazol-2-ylthio]lincomycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 941586-45-4
(7S)-7-deoxy-7-[5-(4,5-difluoro-2-nitrophenyl)-1,3,4-thiadiazol-2-ylthio]lincomycin

: 124-40-3
dimethyl amine

: 941586-78-3
(7S)-7-deoxy-7-[5-(5-dimethylamino-4-fluoro-2-nitrophenyl)-1,3,4-thiadiazol-2-ylthio]lincomycin

Guidance literature:: In methanol; at 50 ℃; for 3.5h; Sealed tube;
DOI:10.1038/ja.2017.59

Reference yield: 83.0%

: 941586-46-5
C₂₆H₃₅F₂N₅O₇S₃*ClH

: 124-40-3
dimethyl amine

: 941586-78-3
(7S)-7-deoxy-7-[5-(5-dimethylamino-4-fluoro-2-nitrophenyl)-1,3,4-thiadiazol-2-ylthio]lincomycin

Guidance literature:: In methanol; at 50 ℃; for 4h;

Reference yield:

: C₃₅H₅₉F₂N₅O₇S₃Si₃

: 941586-78-3
(7S)-7-deoxy-7-[5-(5-dimethylamino-4-fluoro-2-nitrophenyl)-1,3,4-thiadiazol-2-ylthio]lincomycin

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / methanol; water / 20 °C

2: methanol / 3.5 h / 50 °C / Sealed tube

With hydrogenchloride; In methanol; water;
DOI:10.1038/ja.2017.59