4-acetyl-2-(3-chlorophenyl)-5-methyl-1-vinyl-2,3-dihydro-1H-1,2,3-triazole

Base Information

Chemical Name:4-acetyl-2-(3-chlorophenyl)-5-methyl-1-vinyl-2,3-dihydro-1H-1,2,3-triazole
CAS No.:1169829-23-5
Molecular Formula:C₁₃H₁₄ClN₃O
Molecular Weight:263.727
Hs Code.:

Synonyms:4-acetyl-2-(3-chlorophenyl)-5-methyl-1-vinyl-2,3-dihydro-1H-1,2,3-triazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetyl-2-(3-chlorophenyl)-5-methyl-1-vinyl-2,3-dihydro-1H-1,2,3-triazole

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Technology Process of 4-acetyl-2-(3-chlorophenyl)-5-methyl-1-vinyl-2,3-dihydro-1H-1,2,3-triazole

There total 4 articles about 4-acetyl-2-(3-chlorophenyl)-5-methyl-1-vinyl-2,3-dihydro-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1169829-10-0
4-acetyl-2-(3-chlorophenyl)-5-methyl-N-(2-hydroxyethyl)-2,3-dihydro-1H-1,2,3-triazole

: 1169829-23-5
4-acetyl-2-(3-chlorophenyl)-5-methyl-1-vinyl-2,3-dihydro-1H-1,2,3-triazole

Guidance literature:: With phosphoric acid; In ethanol; Reflux;
DOI:10.1007/s00044-009-9215-7

Reference yield:

: 75304-22-2
pentane-2,3,4-trione 3-[(3-chloro-phenyl)-hydrazone]

: 1169829-23-5
4-acetyl-2-(3-chlorophenyl)-5-methyl-1-vinyl-2,3-dihydro-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate / ethanol / 0.5 h / 20 °C

2: phosphoric acid / ethanol / Reflux

With phosphoric acid; potassium acetate; In ethanol;
DOI:10.1007/s00044-009-9215-7

Reference yield:

: 108-42-9
3-chloro-aniline

: 1169829-23-5
4-acetyl-2-(3-chlorophenyl)-5-methyl-1-vinyl-2,3-dihydro-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; sodium nitrite / water / 0 - 5 °C

1.2: 0 - 5 °C

2.1: potassium acetate / ethanol / 0.5 h / 20 °C

3.1: phosphoric acid / ethanol / Reflux

With hydrogenchloride; phosphoric acid; potassium acetate; sodium nitrite; In ethanol; water;
DOI:10.1007/s00044-009-9215-7