4-(4-Chloro-phenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidine-6-thiol

Base Information

• Chemical Name: 4-(4-Chloro-phenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidine-6-thiol
• CAS No.: 106924-32-7
• Molecular Formula: C₁₈H₁₃ClN₄S
• Molecular Weight: 352.847

Synonyms:4-(4-Chloro-phenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidine-6-thiol

Chemical Property of 4-(4-Chloro-phenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidine-6-thiol

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Technology Process of 4-(4-Chloro-phenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidine-6-thiol

There total 1 articles about 4-(4-Chloro-phenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidine-6-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4-chlorobenzaldehyde (104-88-1) + thiourea (17356-08-0) + edaravone (89-25-8) → 4-(4-Chloro-phenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidine-6-thiol (106924-32-7)

Guidance literature:

With acetic acid; at 80 - 85 ℃; for 8h;

DOI:10.1007/s00044-011-9911-y

Reference yield: 80.0%

4-(4-Chloro-phenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidine-6-thiol (106924-32-7) → 2-[4-(4-chlorophenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-yl]-hydrazine (1353388-98-3)

Guidance literature:

With hydrazine hydrate; In 1,4-dioxane; for 10h; Reflux;

DOI:10.1007/s00044-011-9911-y

Reference yield: 72.0%

4-(4-Chloro-phenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidine-6-thiol (106924-32-7) + methyl iodide (74-88-4) → 4-(4-Chloro-phenyl)-3-methyl-6-methylsulfanyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidine

Guidance literature:

With potassium carbonate; In acetone; for 5h; Heating;

upstream raw materials:

4-chlorobenzaldehyde

thiourea

edaravone

Downstream raw materials:

2-((4-(4-chlorophenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-yl)thio)acetyl chloride

4-(4-chlorophenyl)-3-methyl-1-phenyl-4,7-dihydropyrazolo[3,4-d]thiazolo[3,2-a]pyrimidin-6(1H)-one

2-((4-(4-chlorophenyl)-3-methyl-1-phenyl-1Hpyrazolo[3,4-d]pyrimidin-6-yl)thio)-1-(4-methoxyphenyl)ethanone

3-(4-chlorophenyl)-2-((4-(4-chlorophenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-yl)thio)-1-(4-methoxyphenyl)prop-2-en-1-one

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