1,3-dimesityl-4,5-bis[3-(triethoxysilyl)propyl]-4,5-dihydroimidazol-1H-ium chloride

Base Information

Chemical Name:1,3-dimesityl-4,5-bis[3-(triethoxysilyl)propyl]-4,5-dihydroimidazol-1H-ium chloride
CAS No.:1365842-33-6
Molecular Formula:C₃₉H₆₇N₂O₆Si₂*Cl
Molecular Weight:751.595
Hs Code.:

Synonyms:1,3-dimesityl-4,5-bis[3-(triethoxysilyl)propyl]-4,5-dihydroimidazol-1H-ium chloride

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Chemical Property of 1,3-dimesityl-4,5-bis[3-(triethoxysilyl)propyl]-4,5-dihydroimidazol-1H-ium chloride

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Technology Process of 1,3-dimesityl-4,5-bis[3-(triethoxysilyl)propyl]-4,5-dihydroimidazol-1H-ium chloride

There total 8 articles about 1,3-dimesityl-4,5-bis[3-(triethoxysilyl)propyl]-4,5-dihydroimidazol-1H-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 64-17-5
ethanol

: 1365842-32-5,863221-34-5
(4S,5R)-4,5-diallyl-1,3-dimesityl-4,5-dihydro-1H-imidazol-3-ium chloride

: 1365842-33-6
1,3-dimesityl-4,5-bis[3-(triethoxysilyl)propyl]-4,5-dihydroimidazol-1H-ium chloride

Guidance literature:: (4S,5R)-4,5-diallyl-1,3-dimesityl-4,5-dihydro-1H-imidazol-3-ium chloride; With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; trichlorosilane; In 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; at 40 ℃; for 20h; Schlenk technique; Inert atmosphere;

ethanol; With triethylamine; at 0 - 20 ℃; for 2h;
DOI:10.1002/ejoc.201402649

Reference yield:

: 64-17-5
ethanol

: C₃₃H₅₅N₂Si₂⁽¹⁺⁾*Cl^(1-)

: 1365842-33-6
1,3-dimesityl-4,5-bis[3-(triethoxysilyl)propyl]-4,5-dihydroimidazol-1H-ium chloride

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.molcata.2012.01.019

Reference yield:

: 1365842-31-4
(4R,5S)-N,N'-dimesitylocta-1,7-diene-4,5-diamine

: 1365842-33-6
1,3-dimesityl-4,5-bis[3-(triethoxysilyl)propyl]-4,5-dihydroimidazol-1H-ium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium chloride / 140 °C

2: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; trichlorosilane / dichloromethane / 20 h / 40 °C / Inert atmosphere

3: triethylamine / dichloromethane / 2 h / 0 - 20 °C

With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; trichlorosilane; ammonium chloride; triethylamine; In dichloromethane;
DOI:10.1016/j.molcata.2012.01.019