2,3,9,10,16,17,23,24-octakis[3,5-di (tert-butyl)-4-hydroxyphenyl]-1,4,8,11,15,18,22,25-octaazaphthalocyanine

Base Information

• Chemical Name: 2,3,9,10,16,17,23,24-octakis[3,5-di (tert-butyl)-4-hydroxyphenyl]-1,4,8,11,15,18,22,25-octaazaphthalocyanine
• CAS No.: 1373213-12-7
• Molecular Formula: C₁₃₆H₁₇₀N₁₆O₈
• Molecular Weight: 2156.95
• Mol file: 1373213-12-7.mol

Synonyms:2,3,9,10,16,17,23,24-octakis[3,5-di (tert-butyl)-4-hydroxyphenyl]-1,4,8,11,15,18,22,25-octaazaphthalocyanine

Chemical Property of 2,3,9,10,16,17,23,24-octakis[3,5-di (tert-butyl)-4-hydroxyphenyl]-1,4,8,11,15,18,22,25-octaazaphthalocyanine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,9,10,16,17,23,24-octakis[3,5-di (tert-butyl)-4-hydroxyphenyl]-1,4,8,11,15,18,22,25-octaazaphthalocyanine

There total 2 articles about 2,3,9,10,16,17,23,24-octakis[3,5-di (tert-butyl)-4-hydroxyphenyl]-1,4,8,11,15,18,22,25-octaazaphthalocyanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2,3,9,10,16,17,23,24-octakis[3,5-di(tert-butyl)-4-hydroxyphenyl]-1,4,8,11,15,18,22,25-octaazaphthalocyaninato magnesium(II) → 2,3,9,10,16,17,23,24-octakis[3,5-di (tert-butyl)-4-hydroxyphenyl]-1,4,8,11,15,18,22,25-octaazaphthalocyanine (1373213-12-7)

Guidance literature:

With toluene-4-sulfonic acid; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1002/chem.201502533

Reference yield:

5,6-bis[3,5-di(tert-butyl)-4-hydroxyphenyl]pyrazine-2,3-dicarbonitrile (1373213-10-5) → 2,3,9,10,16,17,23,24-octakis[3,5-di (tert-butyl)-4-hydroxyphenyl]-1,4,8,11,15,18,22,25-octaazaphthalocyanine (1373213-12-7)

Guidance literature:

With lithium; In hexan-1-ol; Reflux;

DOI:10.1039/c2cc30712j

Reference yield: 54.0%

2,3,9,10,16,17,23,24-octakis[3,5-di (tert-butyl)-4-hydroxyphenyl]-1,4,8,11,15,18,22,25-octaazaphthalocyanine (1373213-12-7) + zinc diacetate (557-34-6) → 2,3,9,10,16,17,23,24-octakis[3,5-di(tert-butyl)-4-hydroxyphenyl]-1,4,8,11,15,18,22,25-octaazaphthalocyaninato zinc(II)

Guidance literature:

In pyridine; for 1h; Reflux;

DOI:10.1002/chem.201502533

upstream raw materials:

5,6-bis[3,5-di(tert-butyl)-4-hydroxyphenyl]pyrazine-2,3-dicarbonitrile