8-[1-chloro-1-(toluene-4-sulfinyl)-ethyl]-7-methyl-1,4-dioxa-spiro[4.5]decan-8-ol

Base Information

Chemical Name:8-[1-chloro-1-(toluene-4-sulfinyl)-ethyl]-7-methyl-1,4-dioxa-spiro[4.5]decan-8-ol
CAS No.:912539-62-9
Molecular Formula:C₁₈H₂₅ClO₄S
Molecular Weight:372.913
Hs Code.:

Synonyms:8-[1-chloro-1-(toluene-4-sulfinyl)-ethyl]-7-methyl-1,4-dioxa-spiro[4.5]decan-8-ol

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Chemical Property of 8-[1-chloro-1-(toluene-4-sulfinyl)-ethyl]-7-methyl-1,4-dioxa-spiro[4.5]decan-8-ol

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Technology Process of 8-[1-chloro-1-(toluene-4-sulfinyl)-ethyl]-7-methyl-1,4-dioxa-spiro[4.5]decan-8-ol

There total 1 articles about 8-[1-chloro-1-(toluene-4-sulfinyl)-ethyl]-7-methyl-1,4-dioxa-spiro[4.5]decan-8-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1-chloroethyl p-tolyl sulfoxide, lithium α-sulfinyl carbanion

: 702-69-2
7-methyl-1,4-dioxa-spiro[4.5]decan-8-one

: 912539-62-9
8-[1-chloro-1-(toluene-4-sulfinyl)-ethyl]-7-methyl-1,4-dioxa-spiro[4.5]decan-8-ol

Guidance literature:: at -70 ℃;
DOI:10.1016/j.tetlet.2006.07.082

Reference yield: 75.0%

: 912539-62-9
8-[1-chloro-1-(toluene-4-sulfinyl)-ethyl]-7-methyl-1,4-dioxa-spiro[4.5]decan-8-ol

: 100-52-7
benzaldehyde

: 9-[hydroxy(phenyl)methyl]-7,9-dimethyl-1,4-dioxaspiro[4.6]undecan-8-one

Guidance literature:: 8-[1-chloro-1-(toluene-4-sulfinyl)-ethyl]-7-methyl-1,4-dioxa-spiro[4.5]decan-8-ol; With tert-butylmagnesium chloride; isopropylmagnesium chloride; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h;

benzaldehyde; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2006.07.082

Reference yield: 73.0%

: 912539-62-9
8-[1-chloro-1-(toluene-4-sulfinyl)-ethyl]-7-methyl-1,4-dioxa-spiro[4.5]decan-8-ol

: 98-88-4
benzoyl chloride

: 9-benzoyl-7,9-dimethyl-1,4-dioxaspiro[4.6]undecan-8-one

Guidance literature:: 8-[1-chloro-1-(toluene-4-sulfinyl)-ethyl]-7-methyl-1,4-dioxa-spiro[4.5]decan-8-ol; With tert-butylmagnesium chloride; isopropylmagnesium chloride; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h;

benzoyl chloride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2006.07.082