7-triethylsilyl-10-deacetyl-10-benzoyloxycarbonyl-13-acetylbaccatin III

Base Information

Chemical Name:7-triethylsilyl-10-deacetyl-10-benzoyloxycarbonyl-13-acetylbaccatin III
CAS No.:848251-58-1
Molecular Formula:C₄₅H₅₈O₁₃Si
Molecular Weight:835.033
Hs Code.:

Synonyms:7-triethylsilyl-10-deacetyl-10-benzoyloxycarbonyl-13-acetylbaccatin III

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Chemical Property of 7-triethylsilyl-10-deacetyl-10-benzoyloxycarbonyl-13-acetylbaccatin III

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Technology Process of 7-triethylsilyl-10-deacetyl-10-benzoyloxycarbonyl-13-acetylbaccatin III

There total 4 articles about 7-triethylsilyl-10-deacetyl-10-benzoyloxycarbonyl-13-acetylbaccatin III which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 160237-44-5
C₄₃H₅₆O₁₂Si

: 848251-58-1
7-triethylsilyl-10-deacetyl-10-benzoyloxycarbonyl-13-acetylbaccatin III

Guidance literature:: With dmap; In dichloromethane; at 25 ℃;
DOI:10.1021/jm049483y

Reference yield:

: 32981-86-5,172018-16-5
10-deacetylbaccatin III

: 848251-58-1
7-triethylsilyl-10-deacetyl-10-benzoyloxycarbonyl-13-acetylbaccatin III

Guidance literature:: Multi-step reaction with 3 steps

1.1: imidazole / dimethylformamide / 25 °C

2.1: LiHMDS / tetrahydrofuran

2.2: tetrahydrofuran / -40 °C

3.1: DMAP / CH₂Cl₂ / 25 °C

With 1H-imidazole; dmap; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm049483y

Reference yield:

: 994-30-9
triethylsilyl chloride

: 848251-58-1
7-triethylsilyl-10-deacetyl-10-benzoyloxycarbonyl-13-acetylbaccatin III

Guidance literature:: Multi-step reaction with 3 steps

1.1: imidazole / dimethylformamide / 25 °C

2.1: LiHMDS / tetrahydrofuran

2.2: tetrahydrofuran / -40 °C

3.1: DMAP / CH₂Cl₂ / 25 °C

With 1H-imidazole; dmap; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm049483y