6-O-benzoyl-1-N-tet-butoxycarbonyl-3,2',6'-triazido-3',4'-dideoxy-3'-enoneamine

Base Information

Chemical Name:6-O-benzoyl-1-N-tet-butoxycarbonyl-3,2',6'-triazido-3',4'-dideoxy-3'-enoneamine
CAS No.:882050-15-9
Molecular Formula:C₂₄H₃₀N₁₀O₇
Molecular Weight:570.565
Hs Code.:

Synonyms:6-O-benzoyl-1-N-tet-butoxycarbonyl-3,2',6'-triazido-3',4'-dideoxy-3'-enoneamine

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Chemical Property of 6-O-benzoyl-1-N-tet-butoxycarbonyl-3,2',6'-triazido-3',4'-dideoxy-3'-enoneamine

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Technology Process of 6-O-benzoyl-1-N-tet-butoxycarbonyl-3,2',6'-triazido-3',4'-dideoxy-3'-enoneamine

There total 5 articles about 6-O-benzoyl-1-N-tet-butoxycarbonyl-3,2',6'-triazido-3',4'-dideoxy-3'-enoneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 882050-14-8
1-N-tet-butoxycarbonyl-3,2',6'-triazido-3',4'-dideoxy-3'-enoneamine

: 98-88-4
benzoyl chloride

: 882050-15-9
6-O-benzoyl-1-N-tet-butoxycarbonyl-3,2',6'-triazido-3',4'-dideoxy-3'-enoneamine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -50 - 0 ℃;
DOI:10.1021/ol0529750

Reference yield:

: 860640-70-6
1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine

: 882050-15-9
6-O-benzoyl-1-N-tet-butoxycarbonyl-3,2',6'-triazido-3',4'-dideoxy-3'-enoneamine

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / DMAP; Et₃N / CH₂Cl₂ / 48 h / 20 °C

2: 84 percent / PMe₃ / toluene / -78 - -10 °C

3: 87 percent / LiOH*H₂O / tetrahydrofuran; H₂O / 0 - 20 °C

4: 99 percent / DIPEA / CH₂Cl₂ / -50 - 0 °C

With dmap; lithium hydroxide; triethylamine; N-ethyl-N,N-diisopropylamine; trimethylphosphane; In tetrahydrofuran; dichloromethane; water; toluene; 2: Staudinger reaction;
DOI:10.1021/ol0529750

Reference yield:

: 882050-12-6
5,6-di-O-(4-chlorobenzoyl)-1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine

: 882050-15-9
6-O-benzoyl-1-N-tet-butoxycarbonyl-3,2',6'-triazido-3',4'-dideoxy-3'-enoneamine

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / PMe₃ / toluene / -78 - -10 °C

2: 87 percent / LiOH*H₂O / tetrahydrofuran; H₂O / 0 - 20 °C

3: 99 percent / DIPEA / CH₂Cl₂ / -50 - 0 °C

With lithium hydroxide; N-ethyl-N,N-diisopropylamine; trimethylphosphane; In tetrahydrofuran; dichloromethane; water; toluene; 1: Staudinger reaction;
DOI:10.1021/ol0529750