p-nitrophenoxycarbonyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:p-nitrophenoxycarbonyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside
CAS No.:1233921-11-3
Molecular Formula:C₂₁H₂₄N₂O₁₃
Molecular Weight:512.427
Hs Code.:

Synonyms:p-nitrophenoxycarbonyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside

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Chemical Property of p-nitrophenoxycarbonyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside

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Technology Process of p-nitrophenoxycarbonyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside

There total 1 articles about p-nitrophenoxycarbonyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 10294-12-9,10353-11-4,70749-28-9,76612-22-1,116559-73-0,147129-68-8,34051-43-9
2-deoxy-2-acetamido-3,4,6-tri-O-acetyl-D-glucopyranose

: 7693-46-1
4-Nitrophenyl chloroformate

: 1233921-11-3
p-nitrophenoxycarbonyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1021/ja101646k

Reference yield: 75.0%

: 1233921-11-3
p-nitrophenoxycarbonyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside

: 201484-12-0
Fmoc-D-Dab(NH₂)-OH

: C₃₄H₃₉N₃O₁₄

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201600657

Reference yield:

: Fmoc-D-Dab(ivDde)-OH

: 1233921-11-3
p-nitrophenoxycarbonyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside

: C₃₂H₂₇N₂O₅Pol

: 104669-73-0
N^α-(tert-butoxycarbonyl)-N^ε-(allyloxycarbonyl)-L-lysine

: 84624-17-9
N-(9-fluorenylmethoxycarbonyl)-D-valine

: 133464-46-7
(S)-2-[((9H-fluoren-9-yl)methoxy)carbonylamino]-5-(allyloxy)-5-oxopentanoic acid

: C₁₀₅H₁₅₉N₁₉O₅₂

Guidance literature:: C₃₂H₂₇N₂O₅Pol; With piperidine; Automated synthesizer; solid phase reaction;

(S)-2-[((9H-fluoren-9-yl)methoxy)carbonylamino]-5-(allyloxy)-5-oxopentanoic acid; With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; Automated synthesizer; solid phase reaction;

Fmoc-D-Dab(ivDde)-OH; p-nitrophenoxycarbonyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside; N^α-(tert-butoxycarbonyl)-N^ε-(allyloxycarbonyl)-L-lysine; N-(9-fluorenylmethoxycarbonyl)-D-valine; Further stages;
DOI:10.1021/ja101646k