bromo 3,4-dimethoxyphenylacetic acid ethyl ester

Base Information

Chemical Name:bromo 3,4-dimethoxyphenylacetic acid ethyl ester
CAS No.:3152-27-0
Molecular Formula:C₁₂H₁₅BrO₄
Molecular Weight:303.153
Hs Code.:

Synonyms:bromo 3,4-dimethoxyphenylacetic acid ethyl ester

Suppliers and Price of bromo 3,4-dimethoxyphenylacetic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of bromo 3,4-dimethoxyphenylacetic acid ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bromo 3,4-dimethoxyphenylacetic acid ethyl ester

There total 5 articles about bromo 3,4-dimethoxyphenylacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 32407-67-3
ethyl-2-(3,4-dimethoxyphenyl)-2-hydroxyacetate

: 3152-27-0
bromo 3,4-dimethoxyphenylacetic acid ethyl ester

Guidance literature:: With phosphorus tribromide; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1055/s-2006-942404

Reference yield: 47.0%

: 18066-68-7
ethyl 3,4-dimethoxyphenylacetate

: 3152-27-0
bromo 3,4-dimethoxyphenylacetic acid ethyl ester

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; Reflux;
DOI:10.1021/ol100522z

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 3152-27-0
bromo 3,4-dimethoxyphenylacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / AlCl₃ / CH₂Cl₂ / 1 h / 20 °C

2: 79 percent / NaBH₄ / ethanol / 0.25 h / -30 °C

3: 89 percent / PBr₃ / CH₂Cl₂ / 1 h / 0 °C

With sodium tetrahydroborate; aluminium trichloride; phosphorus tribromide; In ethanol; dichloromethane; 1: Friedel-Crafts acylation;
DOI:10.1055/s-2006-942404