(1-(4-(thiophen-2-yl)thiazol-2-yl)-1H-1,2,3-triazol-4-yl)methyl (E)-cinnamate

Base Information

Chemical Name:(1-(4-(thiophen-2-yl)thiazol-2-yl)-1H-1,2,3-triazol-4-yl)methyl (E)-cinnamate
CAS No.:1258795-43-5
Molecular Formula:C₁₉H₁₄N₄O₂S₂
Molecular Weight:394.478
Hs Code.:

Synonyms:(1-(4-(thiophen-2-yl)thiazol-2-yl)-1H-1,2,3-triazol-4-yl)methyl (E)-cinnamate

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Chemical Property of (1-(4-(thiophen-2-yl)thiazol-2-yl)-1H-1,2,3-triazol-4-yl)methyl (E)-cinnamate

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Technology Process of (1-(4-(thiophen-2-yl)thiazol-2-yl)-1H-1,2,3-triazol-4-yl)methyl (E)-cinnamate

There total 4 articles about (1-(4-(thiophen-2-yl)thiazol-2-yl)-1H-1,2,3-triazol-4-yl)methyl (E)-cinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 91368-35-3,29584-63-2
prop-2-ynyl 3-phenylacrylate

: 1125409-90-6
C₇H₄BrNS₂

: 1258795-43-5
(1-(4-(thiophen-2-yl)thiazol-2-yl)-1H-1,2,3-triazol-4-yl)methyl (E)-cinnamate

Guidance literature:: With copper(l) iodide; sodium azide; N,N`-dimethylethylenediamine; In N,N-dimethyl-formamide; at 60 ℃; for 6h; Darkness; Inert atmosphere;
DOI:10.1021/co1000234

Reference yield:

: 43045-25-6
2-thiocyanato-1-(thiophen-2-yl)ethanone

: 1258795-43-5
(1-(4-(thiophen-2-yl)thiazol-2-yl)-1H-1,2,3-triazol-4-yl)methyl (E)-cinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide; acetic acid / water

2: copper(l) iodide; sodium azide; N,N`-dimethylethylenediamine / N,N-dimethyl-formamide / 6 h / 60 °C / Darkness; Inert atmosphere

With copper(l) iodide; sodium azide; hydrogen bromide; acetic acid; N,N`-dimethylethylenediamine; In water; N,N-dimethyl-formamide;
DOI:10.1021/co1000234

Reference yield:

: 88-15-3,97511-16-5
2-Acetylthiophene

: 1258795-43-5
(1-(4-(thiophen-2-yl)thiazol-2-yl)-1H-1,2,3-triazol-4-yl)methyl (E)-cinnamate

Guidance literature:: Multi-step reaction with 4 steps

1: bromine / 1,4-dioxane; diethyl ether

2: N,N-dimethyl-formamide

3: hydrogen bromide; acetic acid / water

4: copper(l) iodide; sodium azide; N,N`-dimethylethylenediamine / N,N-dimethyl-formamide / 6 h / 60 °C / Darkness; Inert atmosphere

With copper(l) iodide; sodium azide; hydrogen bromide; bromine; acetic acid; N,N`-dimethylethylenediamine; In 1,4-dioxane; diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/co1000234