(4S)-3-[3-(3-carboxy-4-methoxyphenyl)-2-ethylpropionyl]-4-benzyl-2-oxazolidinone

Base Information

Chemical Name:(4S)-3-[3-(3-carboxy-4-methoxyphenyl)-2-ethylpropionyl]-4-benzyl-2-oxazolidinone
CAS No.:311771-00-3
Molecular Formula:C₂₃H₂₅NO₆
Molecular Weight:411.455
Hs Code.:

Synonyms:(4S)-3-[3-(3-carboxy-4-methoxyphenyl)-2-ethylpropionyl]-4-benzyl-2-oxazolidinone

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Chemical Property of (4S)-3-[3-(3-carboxy-4-methoxyphenyl)-2-ethylpropionyl]-4-benzyl-2-oxazolidinone

Chemical Property:

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Technology Process of (4S)-3-[3-(3-carboxy-4-methoxyphenyl)-2-ethylpropionyl]-4-benzyl-2-oxazolidinone

There total 4 articles about (4S)-3-[3-(3-carboxy-4-methoxyphenyl)-2-ethylpropionyl]-4-benzyl-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (4S)-3-[3-(3-benzyloxycarbonyl-4-methoxyphenyl)-2-ethyl-3-hydroxypropionyl]-4-benzyl-2-oxazolidinone

: 311771-00-3
(4S)-3-[3-(3-carboxy-4-methoxyphenyl)-2-ethylpropionyl]-4-benzyl-2-oxazolidinone

Guidance literature:: With triethylsilane; sodium hydroxide; trifluoroacetic acid;

Reference yield:

: 84923-70-6
5-formyl-2-methoxybenzoic acid

: 311771-00-3
(4S)-3-[3-(3-carboxy-4-methoxyphenyl)-2-ethylpropionyl]-4-benzyl-2-oxazolidinone

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 4 h / 20 °C

2.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / 1.58 h / -74 - 0 °C

2.2: 3.83 h / -75 - 0 °C

2.3: phosphate buffer / 0.5 h / 0 °C

3.1: triethylsilane; trifluoroacetic acid / 98.4 h / 0 - 20 °C

With triethylsilane; di-n-butylboryl trifluoromethanesulfonate; potassium hydrogencarbonate; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 111292-87-6,143097-11-4,112459-79-7
(S)-4-benzyl-3-butyryloxazolidin-2-one

: 311771-00-3
(4S)-3-[3-(3-carboxy-4-methoxyphenyl)-2-ethylpropionyl]-4-benzyl-2-oxazolidinone

Guidance literature:: Multi-step reaction with 2 steps

1.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / 1.58 h / -74 - 0 °C

1.2: 3.83 h / -75 - 0 °C

1.3: phosphate buffer / 0.5 h / 0 °C

2.1: triethylsilane; trifluoroacetic acid / 98.4 h / 0 - 20 °C

With triethylsilane; di-n-butylboryl trifluoromethanesulfonate; triethylamine; trifluoroacetic acid; In dichloromethane;