O,O'-bis(tert-butyldimethylsilyl)-4-(1,2-dideoxy-β-D-ribofuranos-1-yl)catechol

Base Information

Chemical Name:O,O'-bis(tert-butyldimethylsilyl)-4-(1,2-dideoxy-β-D-ribofuranos-1-yl)catechol
CAS No.:307003-27-6
Molecular Formula:C₂₃H₄₂O₅Si₂
Molecular Weight:454.754
Hs Code.:

Synonyms:O,O'-bis(tert-butyldimethylsilyl)-4-(1,2-dideoxy-β-D-ribofuranos-1-yl)catechol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O,O'-bis(tert-butyldimethylsilyl)-4-(1,2-dideoxy-β-D-ribofuranos-1-yl)catechol

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Technology Process of O,O'-bis(tert-butyldimethylsilyl)-4-(1,2-dideoxy-β-D-ribofuranos-1-yl)catechol

There total 6 articles about O,O'-bis(tert-butyldimethylsilyl)-4-(1,2-dideoxy-β-D-ribofuranos-1-yl)catechol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 307003-25-4
O,O'-bis(tert-butyldimethylsilyl)-4-[1,2-dideoxy-3,5-O,O'-bis(ethoxycarbonyl)-β-D-ribofuranos-1-yl]catechol

: 307003-27-6
O,O'-bis(tert-butyldimethylsilyl)-4-(1,2-dideoxy-β-D-ribofuranos-1-yl)catechol

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 0.833333h;
DOI:10.1016/S0928-0987(00)00210-4

Reference yield:

: 153185-80-9
1,2-bis((tert-butyldimethylsilyl)oxy)benzene

: 307003-27-6
O,O'-bis(tert-butyldimethylsilyl)-4-(1,2-dideoxy-β-D-ribofuranos-1-yl)catechol

Guidance literature:: Multi-step reaction with 2 steps

1: 36 percent / SnCl₄ / CH₂Cl₂ / 0.25 h / 0 °C

2: 84 percent / K₂CO₃ / methanol / 0.83 h / 20 °C

With tin(IV) chloride; potassium carbonate; In methanol; dichloromethane; 1: Friedel-Crafts coupling reaction;
DOI:10.1016/S0928-0987(00)00210-4

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 307003-27-6
O,O'-bis(tert-butyldimethylsilyl)-4-(1,2-dideoxy-β-D-ribofuranos-1-yl)catechol

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / pyridine / 48 h / 80 °C

2: 36 percent / SnCl₄ / CH₂Cl₂ / 0.25 h / 0 °C

3: 84 percent / K₂CO₃ / methanol / 0.83 h / 20 °C

With pyridine; tin(IV) chloride; potassium carbonate; In methanol; dichloromethane; 2: Friedel-Crafts coupling reaction;
DOI:10.1016/S0928-0987(00)00210-4