tert-butyl 6-benzyloxycarbonylamino-3-(2-formylfuran-3-yl)-2-hydroxybenzoate

Base Information

Chemical Name:tert-butyl 6-benzyloxycarbonylamino-3-(2-formylfuran-3-yl)-2-hydroxybenzoate
CAS No.:1356112-87-2
Molecular Formula:C₂₄H₂₃NO₇
Molecular Weight:437.449
Hs Code.:

Synonyms:tert-butyl 6-benzyloxycarbonylamino-3-(2-formylfuran-3-yl)-2-hydroxybenzoate

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Chemical Property of tert-butyl 6-benzyloxycarbonylamino-3-(2-formylfuran-3-yl)-2-hydroxybenzoate

Chemical Property:

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Technology Process of tert-butyl 6-benzyloxycarbonylamino-3-(2-formylfuran-3-yl)-2-hydroxybenzoate

There total 5 articles about tert-butyl 6-benzyloxycarbonylamino-3-(2-formylfuran-3-yl)-2-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356112-88-3
tert-butyl 6-amino-3-(2-formylfuran-3-yl)-2-hydroxybenzoate

: 501-53-1,94274-21-2
benzyl chloroformate

: 1356112-87-2
tert-butyl 6-benzyloxycarbonylamino-3-(2-formylfuran-3-yl)-2-hydroxybenzoate

Guidance literature:: In diethyl ether; at 20 ℃; for 2h;

Reference yield:

: 681247-11-0
methyl 6-amino-3-bromo-2-hydroxybenzoate

: 1356112-87-2
tert-butyl 6-benzyloxycarbonylamino-3-(2-formylfuran-3-yl)-2-hydroxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: water; lithium hydroxide monohydrate / 1,4-dioxane / 5 h / 80 - 100 °C

2: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 4 h / 20 °C

3: caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane; water / 3 h / 70 °C / Inert atmosphere

4: diethyl ether / 2 h / 20 °C

With dmap; lithium hydroxide monohydrate; water; caesium carbonate; dicyclohexyl-carbodiimide; tri tert-butylphosphoniumtetrafluoroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; diethyl ether; water;

Reference yield:

: 1055881-23-6
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)furan-2-carbaldehyde

: 1356112-87-2
tert-butyl 6-benzyloxycarbonylamino-3-(2-formylfuran-3-yl)-2-hydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane; water / 3 h / 70 °C / Inert atmosphere

2: diethyl ether / 2 h / 20 °C

With caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In 1,4-dioxane; diethyl ether; water;