ethyl exo-bicyclo<4.1.0>heptyl-7-glyoxylate

Base Information

Chemical Name:ethyl exo-bicyclo<4.1.0>heptyl-7-glyoxylate
CAS No.:61558-26-7
Molecular Formula:C₁₁H₁₆O₃
Molecular Weight:196.246
Hs Code.:

Synonyms:ethyl exo-bicyclo<4.1.0>heptyl-7-glyoxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl exo-bicyclo<4.1.0>heptyl-7-glyoxylate

Chemical Property:

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Technology Process of ethyl exo-bicyclo<4.1.0>heptyl-7-glyoxylate

There total 1 articles about ethyl exo-bicyclo<4.1.0>heptyl-7-glyoxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14214-10-9
ethyl diazopyruvate

: 110-83-8
cyclohexene

: 61558-27-8
ethyl 2-cyclohexenylpyruvate

: 61558-26-7
ethyl exo-bicyclo<4.1.0>heptyl-7-glyoxylate

Guidance literature:: With copper; In xylene; at 100 ℃; for 0.25h; Yield given. Yields of byproduct given;
DOI:10.1021/ja00345a059

Reference yield:

: 61558-26-7
ethyl exo-bicyclo<4.1.0>heptyl-7-glyoxylate

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: C₁₈H₂₄N₂O₄S

Guidance literature:: In toluene; at 120 ℃;
DOI:10.1002/anie.200803910

Reference yield:

: 61558-26-7
ethyl exo-bicyclo<4.1.0>heptyl-7-glyoxylate

: 21448-77-1
(1α,6α,7α)-bicyclo[4.1.0]heptane-7-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / Heating

2: (i) Pb(OAc)4, (ii) Ag₂O

With lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1021/jo00444a052