2-[4-methoxy-3-(trifluoromethyl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-[4-methoxy-3-(trifluoromethyl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1445019-24-8
Molecular Formula:C₁₄H₁₈BF₃O₃
Molecular Weight:302.101
Hs Code.:

Synonyms:2-[4-methoxy-3-(trifluoromethyl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Suppliers and Price of 2-[4-methoxy-3-(trifluoromethyl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 2-[4-methoxy-3-(trifluoromethyl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 2-[4-methoxy-3-(trifluoromethyl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 3 articles about 2-[4-methoxy-3-(trifluoromethyl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.4%

: 1514-11-0
4-bromo-1-methoxy-2-(trifluoromethyl)benzene

: 73183-34-3
bis(pinacol)diborane

: 1445019-24-8
2-[4-methoxy-3-(trifluoromethyl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 100 ℃; for 1h; Inert atmosphere;

Reference yield:

: 395-48-2
1-methoxy-2-(trifluoromethyl)benzene

: 73183-34-3
bis(pinacol)diborane

: 1445019-24-8
2-[4-methoxy-3-(trifluoromethyl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: C₁₅H₂₁BF₂O₃

Guidance literature:: With C₃₉H₅₉Br₂CoN₇Si₂; sodium triethylborohydride; cyclohexene; In tetrahydrofuran; at 100 ℃; for 36h; Overall yield = 95 %; Overall yield = 143 mg; regioselective reaction; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1002/chem.201605937