Benzoic acid, 2-(acetylaMino)-3-Methyl-, Methyl ester

Base Information

Chemical Name:Benzoic acid, 2-(acetylaMino)-3-Methyl-, Methyl ester
CAS No.:37619-23-1
Molecular Formula:C₁₁H₁₃NO₃
Molecular Weight:207.229
Hs Code.:
Mol file:37619-23-1.mol

Synonyms:2-acetylamino-3-methyl-benzoic acid methyl ester

Suppliers and Price of Benzoic acid, 2-(acetylaMino)-3-Methyl-, Methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
METHYL 2-ACETAMIDO-3-METHYLBENZOATE 95.00%
5MG
$ 498.63

Total 2 raw suppliers

Chemical Property of Benzoic acid, 2-(acetylaMino)-3-Methyl-, Methyl ester

Chemical Property:

Melting Point:116 °C(Solv: methanol (67-56-1))
Boiling Point:370.0±30.0 °C(Predicted)
PKA:14.52±0.70(Predicted)
Density:1.172±0.06 g/cm3(Predicted)

Purity/Quality:

More than 98% ^*data from raw suppliers

METHYL 2-ACETAMIDO-3-METHYLBENZOATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 2-(acetylaMino)-3-Methyl-, Methyl ester

There total 2 articles about Benzoic acid, 2-(acetylaMino)-3-Methyl-, Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22223-49-0
methyl 2-amino-3-methylbenzoate

: 108-24-7
acetic anhydride

: 37619-23-1
2-acetylamino-3-methyl-benzoic acid methyl ester

Guidance literature:: In chloroform; at 20 - 40 ℃; for 1h;

Reference yield:

: 4389-45-1
3-methylantranilic acid

: 37619-23-1
2-acetylamino-3-methyl-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0.67 h / 20 °C

1.2: 20 °C

2.1: chloroform / 1 h / 20 - 40 °C

With caesium carbonate; In chloroform; N,N-dimethyl-formamide;

Reference yield:

: 37619-23-1
2-acetylamino-3-methyl-benzoic acid methyl ester

: 1031413-43-0
1'-(1H-indazol-7-ylcarbonyl)-6,7-dimethylspiro[chromene-2,4'-piperidin]-4(3H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium acetate; isopentyl nitrite / chloroform / Heating / reflux

2.1: potassium hydroxide; water / methanol / 0 - 20 °C / Heating / reflux

2.2: pH 5.5

3.1: triethylamine; HATU / dichloromethane / 16 h / 20 °C

With potassium hydroxide; water; potassium acetate; triethylamine; HATU; isopentyl nitrite; In methanol; dichloromethane; chloroform;