tert-butyl 2-(4-(((2-methoxy-6-phenylpyridin-3-yl)methyl)amino)-phenoxy)ethanoate

Base Information

Chemical Name:tert-butyl 2-(4-(((2-methoxy-6-phenylpyridin-3-yl)methyl)amino)-phenoxy)ethanoate
CAS No.:1202164-04-2
Molecular Formula:C₂₅H₂₈N₂O₄
Molecular Weight:420.508
Hs Code.:

Synonyms:tert-butyl 2-(4-(((2-methoxy-6-phenylpyridin-3-yl)methyl)amino)-phenoxy)ethanoate

Suppliers and Price of tert-butyl 2-(4-(((2-methoxy-6-phenylpyridin-3-yl)methyl)amino)-phenoxy)ethanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 2-(4-(((2-methoxy-6-phenylpyridin-3-yl)methyl)amino)-phenoxy)ethanoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of tert-butyl 2-(4-(((2-methoxy-6-phenylpyridin-3-yl)methyl)amino)-phenoxy)ethanoate

There total 5 articles about tert-butyl 2-(4-(((2-methoxy-6-phenylpyridin-3-yl)methyl)amino)-phenoxy)ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1202163-75-4
2-methoxy-6-phenylnicotinaldehyde

: 167843-57-4
tert-butyl 2-(4-aminophenoxy)acetate

: 1202164-04-2
tert-butyl 2-(4-(((2-methoxy-6-phenylpyridin-3-yl)methyl)amino)-phenoxy)ethanoate

Guidance literature:: 2-methoxy-6-phenylnicotinaldehyde; tert-butyl 2-(4-aminophenoxy)acetate; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

With sodium tris(acetoxy)borohydride; In dichloromethane; Inert atmosphere;

Reference yield:

: 125031-47-2
Methyl 1,2-Dihydro-2-oxo-6-phenyl-3-pyridinecarboxylate

: 1202164-04-2
tert-butyl 2-(4-(((2-methoxy-6-phenylpyridin-3-yl)methyl)amino)-phenoxy)ethanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: silver(l) oxide / toluene / 50 - 70 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

3.1: pyridinium chlorochromate / dichloromethane / 20 °C

4.1: dichloromethane / 1 h / 20 °C / Inert atmosphere

4.2: Inert atmosphere

With lithium aluminium tetrahydride; pyridinium chlorochromate; silver(l) oxide; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 85815-01-6
methyl 2-methoxy-6-phenyl-pyridine-3-carboxylate

: 1202164-04-2
tert-butyl 2-(4-(((2-methoxy-6-phenylpyridin-3-yl)methyl)amino)-phenoxy)ethanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2.1: pyridinium chlorochromate / dichloromethane / 20 °C

3.1: dichloromethane / 1 h / 20 °C / Inert atmosphere

3.2: Inert atmosphere

With lithium aluminium tetrahydride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;