2-(4-(((2-methoxy-6-phenylpyridin-3yl)methyl)amino)phenoxy)ethanoic acid

Base Information

Chemical Name:2-(4-(((2-methoxy-6-phenylpyridin-3yl)methyl)amino)phenoxy)ethanoic acid
CAS No.:1202162-73-9
Molecular Formula:C₂₁H₂₀N₂O₄
Molecular Weight:364.401
Hs Code.:

Synonyms:2-(4-(((2-methoxy-6-phenylpyridin-3yl)methyl)amino)phenoxy)ethanoic acid

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Chemical Property of 2-(4-(((2-methoxy-6-phenylpyridin-3yl)methyl)amino)phenoxy)ethanoic acid

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Technology Process of 2-(4-(((2-methoxy-6-phenylpyridin-3yl)methyl)amino)phenoxy)ethanoic acid

There total 5 articles about 2-(4-(((2-methoxy-6-phenylpyridin-3yl)methyl)amino)phenoxy)ethanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1202164-04-2
tert-butyl 2-(4-(((2-methoxy-6-phenylpyridin-3-yl)methyl)amino)-phenoxy)ethanoate

: 1202162-73-9
2-(4-(((2-methoxy-6-phenylpyridin-3yl)methyl)amino)phenoxy)ethanoic acid

Guidance literature:: tert-butyl 2-(4-(((2-methoxy-6-phenylpyridin-3-yl)methyl)amino)-phenoxy)ethanoate; With trifluoroacetic acid; In dichloromethane; at 20 ℃;

With sodium hydroxide; In water; for 0.5h;

With citric acid; In water;

Reference yield:

: 125031-47-2
Methyl 1,2-Dihydro-2-oxo-6-phenyl-3-pyridinecarboxylate

: 1202162-73-9
2-(4-(((2-methoxy-6-phenylpyridin-3yl)methyl)amino)phenoxy)ethanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: silver(l) oxide / toluene / 50 - 70 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

3.1: pyridinium chlorochromate / dichloromethane / 20 °C

4.1: dichloromethane / 1 h / 20 °C / Inert atmosphere

4.2: Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 20 °C

5.2: 0.5 h

With lithium aluminium tetrahydride; pyridinium chlorochromate; trifluoroacetic acid; silver(l) oxide; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 85815-01-6
methyl 2-methoxy-6-phenyl-pyridine-3-carboxylate

: 1202162-73-9
2-(4-(((2-methoxy-6-phenylpyridin-3yl)methyl)amino)phenoxy)ethanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2.1: pyridinium chlorochromate / dichloromethane / 20 °C

3.1: dichloromethane / 1 h / 20 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 20 °C

4.2: 0.5 h

With lithium aluminium tetrahydride; pyridinium chlorochromate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;