4,6-di-O-acetyl-1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

Base Information

Chemical Name:4,6-di-O-acetyl-1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin
CAS No.:959918-94-6
Molecular Formula:C₈₁H₉₀N₆O₂₄
Molecular Weight:1531.63
Hs Code.:

Synonyms:4,6-di-O-acetyl-1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

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Chemical Property of 4,6-di-O-acetyl-1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

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Technology Process of 4,6-di-O-acetyl-1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

There total 1 articles about 4,6-di-O-acetyl-1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 959918-87-7
4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose

: 959918-92-4
1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine

: 959918-94-6
4,6-di-O-acetyl-1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

Guidance literature:: 4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose; 1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine; In dichloromethane; at 20 ℃; for 1h; Molecular sieve;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 - 20 ℃; for 3h; light shielding;

With triethylamine; In dichloromethane; at 0 ℃;

Reference yield:

: 959918-94-6
4,6-di-O-acetyl-1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

: 959918-93-5
1-N-[(S)-3-amino-N-benzyloxycarbonyl-2-hydroxypropionyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

Guidance literature:: 4",6"-di-O-acetyl-1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2,2"-di-O-benzyl-3,2',6',3"-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin; With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 1h;

With sodium methylate; In methanol; chloroform; at 0 - 20 ℃; for 2h;

With acetic acid; In methanol; chloroform; at 0 ℃;