1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine

Base Information

Chemical Name:1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine
CAS No.:959918-92-4
Molecular Formula:C₅₆H₆₃N₅O₁₆
Molecular Weight:1062.14
Hs Code.:

Synonyms:1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine

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Chemical Property of 1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine

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Technology Process of 1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine

There total 1 articles about 1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 959919-65-4
(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropanoic acid

: 959918-81-1
2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine

: 959918-92-4
1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine

Guidance literature:: With 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In tetrahydrofuran; water; isopropyl alcohol; at 20 ℃; for 1h;

Reference yield:

: 959918-87-7
4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose

: 959918-92-4
1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine

: 959918-94-6
4,6-di-O-acetyl-1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

Guidance literature:: 4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose; 1-N-[(S)-2-acetoxy-3-amino-N-benzyloxycarbonylpropionyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine; In dichloromethane; at 20 ℃; for 1h; Molecular sieve;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 - 20 ℃; for 3h; light shielding;

With triethylamine; In dichloromethane; at 0 ℃;