N-[2-(benzyloxy)-5-((1R)-2-bromo-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)phenyl]-dimethanesulfonamide

Base Information

Chemical Name:N-[2-(benzyloxy)-5-((1R)-2-bromo-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)phenyl]-dimethanesulfonamide
CAS No.:921598-09-6
Molecular Formula:C₂₃H₃₄BrNO₆S₂Si
Molecular Weight:592.648
Hs Code.:

Synonyms:N-[2-(benzyloxy)-5-((1R)-2-bromo-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)phenyl]-dimethanesulfonamide

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Chemical Property of N-[2-(benzyloxy)-5-((1R)-2-bromo-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)phenyl]-dimethanesulfonamide

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Technology Process of N-[2-(benzyloxy)-5-((1R)-2-bromo-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)phenyl]-dimethanesulfonamide

There total 1 articles about N-[2-(benzyloxy)-5-((1R)-2-bromo-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)phenyl]-dimethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 861448-71-7
N-[2-(benzyloxy)-5-((1R)-2-bromo-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)phenyl]methane sulfonamide

: 124-63-0
methanesulfonyl chloride

: 921598-09-6
N-[2-(benzyloxy)-5-((1R)-2-bromo-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)phenyl]-dimethanesulfonamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 5 ℃; for 1.16667h;
DOI:10.1021/op2002408

Reference yield: 73.0%

: 921598-09-6
N-[2-(benzyloxy)-5-((1R)-2-bromo-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)phenyl]-dimethanesulfonamide

: 921598-10-9
N-{2-(benzyloxy)-5-[(1R)-2-bromo-1-hydroxyethyl]phenyl}-N-(methylsulfonyl)methanesulfonamide

Guidance literature:: With triethylamine tris(hydrogen fluoride); In tetrahydrofuran; methanol; at 20 ℃; for 30h;
DOI:10.1021/op2002408

Reference yield:

: 921598-09-6
N-[2-(benzyloxy)-5-((1R)-2-bromo-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)phenyl]-dimethanesulfonamide

: 921598-12-1
N-{2-(benzyloxy)-5-[(2R)-oxiran-2-yl]phenyl}-N-(methylsulfonyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran; methanol / 30 h / 20 °C

2: potassium carbonate / tetrahydrofuran; methanol / 18 h / 20 °C

With potassium carbonate; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; methanol;
DOI:10.1021/op2002408