Technology Process of C25H36O3Si
There total 9 articles about C25H36O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 0 - 20 ℃;
for 4h;
DOI:10.1002/hlca.201300221
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: nickel(II) chloride hexahydrate; sodium tetrahydroborate / methanol / 0.02 h / 0 - 20 °C
2.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.17 h / -78 °C
3.1: D-Prolin / dimethyl sulfoxide / 0.5 h / 0 - 20 °C
3.2: 2 h / 20 °C
4.1: copper(ll) sulfate pentahydrate / methanol / 0 - 20 °C
5.1: di(n-butyl)tin oxide; triethylamine / dichloromethane / 4 h / 0 - 20 °C
6.1: potassium carbonate / methanol / 1 h / 20 °C
7.1: copper(l) iodide / tetrahydrofuran / 1 h / -20 °C / Inert atmosphere
8.1: 1H-imidazole / dichloromethane / 4 h / 0 - 20 °C
9.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 0 - 20 °C
With
1H-imidazole; sodium tetrahydroborate; copper(l) iodide; copper(ll) sulfate pentahydrate; nickel(II) chloride hexahydrate; diisobutylaluminium hydride; di(n-butyl)tin oxide; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; D-Prolin;
In
tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1002/hlca.201300221
- Guidance literature:
-
Multi-step reaction with 6 steps
1: copper(ll) sulfate pentahydrate / methanol / 0 - 20 °C
2: di(n-butyl)tin oxide; triethylamine / dichloromethane / 4 h / 0 - 20 °C
3: potassium carbonate / methanol / 1 h / 20 °C
4: copper(l) iodide / tetrahydrofuran / 1 h / -20 °C / Inert atmosphere
5: 1H-imidazole / dichloromethane / 4 h / 0 - 20 °C
6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 0 - 20 °C
With
1H-imidazole; copper(l) iodide; copper(ll) sulfate pentahydrate; di(n-butyl)tin oxide; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/hlca.201300221