N-phenyl-N'-(2,4,6-trimethylphenyl)-1H-benzotriazole-1-carboximidamide

Base Information

• Chemical Name: N-phenyl-N'-(2,4,6-trimethylphenyl)-1H-benzotriazole-1-carboximidamide
• CAS No.: 865073-52-5
• Molecular Formula: C₂₂H₂₁N₅
• Molecular Weight: 355.442
• Mol file: 865073-52-5.mol

Synonyms:N-phenyl-N'-(2,4,6-trimethylphenyl)-1H-benzotriazole-1-carboximidamide

Chemical Property of N-phenyl-N'-(2,4,6-trimethylphenyl)-1H-benzotriazole-1-carboximidamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-phenyl-N'-(2,4,6-trimethylphenyl)-1H-benzotriazole-1-carboximidamide

There total 4 articles about N-phenyl-N'-(2,4,6-trimethylphenyl)-1H-benzotriazole-1-carboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1-(N-phenylthiocarbamoyl)-1H-benzotriazole (24694-06-2) + [(2,4,6-trimethylphenyl)imino](triphenyl)phosphorane (86133-53-1) → N-phenyl-N'-(2,4,6-trimethylphenyl)-1H-benzotriazole-1-carboximidamide (865073-52-5)

Guidance literature:

In toluene; at 110 ℃; for 1h;

DOI:10.1002/hlca.200590131

Reference yield:

2,4,6-trimethylaniline azide (14213-00-4) → N-phenyl-N'-(2,4,6-trimethylphenyl)-1H-benzotriazole-1-carboximidamide (865073-52-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / diethyl ether / 2 h / Heating

2: 80 percent / toluene / 1 h / 110 °C

In diethyl ether; toluene;

DOI:10.1002/hlca.200590131

Reference yield:

aniline (62-53-3) → N-phenyl-N'-(2,4,6-trimethylphenyl)-1H-benzotriazole-1-carboximidamide (865073-52-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / CH₂Cl₂ / 18 h / 20 °C

2: 80 percent / toluene / 1 h / 110 °C

In dichloromethane; toluene;

DOI:10.1002/hlca.200590131

upstream raw materials:

1-(N-phenylthiocarbamoyl)-1H-benzotriazole

[(2,4,6-trimethylphenyl)imino](triphenyl)phosphorane

2,4,6-trimethylaniline azide

aniline