C₂₅H₃₂N₂O₇

Base Information

Chemical Name:C₂₅H₃₂N₂O₇
CAS No.:1609453-81-7
Molecular Formula:C₂₅H₃₂N₂O₇
Molecular Weight:472.538
Hs Code.:

C<sub>25</sub>H<sub>32</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₂₅H₃₂N₂O₇

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Chemical Property of C₂₅H₃₂N₂O₇

Chemical Property:

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Technology Process of C₂₅H₃₂N₂O₇

There total 5 articles about C₂₅H₃₂N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1609453-79-3
C₂₃H₂₇NO₇

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1609453-81-7
C₂₅H₃₂N₂O₇

Guidance literature:: C₂₃H₂₇NO₇; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

N,O-dimethylhydroxylamine*hydrochloride; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo500493c

Reference yield:

: 90-96-0
bis(p-methoxyphenyl)methanone

: 1609453-81-7
C₂₅H₃₂N₂O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / methanol / 30 h / 20 °C / Inert atmosphere

2.1: (1S)-10-camphorsulfonic acid / toluene / 5 h / Reflux; Inert atmosphere

3.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 °C / Inert atmosphere

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

4.2: 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; sulfuric acid; (1S)-10-camphorsulfonic acid; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/jo500493c

Reference yield:

: 2186-93-8
4,4’-dimethoxybenzophenone dimethyl acetal

: 1609453-81-7
C₂₅H₃₂N₂O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: (1S)-10-camphorsulfonic acid / toluene / 5 h / Reflux; Inert atmosphere

2.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 °C / Inert atmosphere

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; (1S)-10-camphorsulfonic acid; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo500493c