[5-Bromo-2-((1R,3R)-3-bromo-2,2-dimethyl-6-methylene-cyclohexylmethyl)-4-methoxy-phenoxy]-tert-butyl-dimethyl-silane

Base Information

Chemical Name:[5-Bromo-2-((1R,3R)-3-bromo-2,2-dimethyl-6-methylene-cyclohexylmethyl)-4-methoxy-phenoxy]-tert-butyl-dimethyl-silane
CAS No.:156170-20-6
Molecular Formula:C₂₃H₃₆Br₂O₂Si
Molecular Weight:532.431
Hs Code.:

Synonyms:[5-Bromo-2-((1R,3R)-3-bromo-2,2-dimethyl-6-methylene-cyclohexylmethyl)-4-methoxy-phenoxy]-tert-butyl-dimethyl-silane

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Chemical Property of [5-Bromo-2-((1R,3R)-3-bromo-2,2-dimethyl-6-methylene-cyclohexylmethyl)-4-methoxy-phenoxy]-tert-butyl-dimethyl-silane

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Technology Process of [5-Bromo-2-((1R,3R)-3-bromo-2,2-dimethyl-6-methylene-cyclohexylmethyl)-4-methoxy-phenoxy]-tert-butyl-dimethyl-silane

There total 1 articles about [5-Bromo-2-((1R,3R)-3-bromo-2,2-dimethyl-6-methylene-cyclohexylmethyl)-4-methoxy-phenoxy]-tert-butyl-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: (3R)-Cyclocymopol monomethyl ether

: 156170-20-6
[5-Bromo-2-((1R,3R)-3-bromo-2,2-dimethyl-6-methylene-cyclohexylmethyl)-4-methoxy-phenoxy]-tert-butyl-dimethyl-silane

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; for 6h; Ambient temperature;
DOI:10.1021/jm950747d

Reference yield: 88.0%

: 156170-20-6
[5-Bromo-2-((1R,3R)-3-bromo-2,2-dimethyl-6-methylene-cyclohexylmethyl)-4-methoxy-phenoxy]-tert-butyl-dimethyl-silane

: 166523-69-9
[5-Bromo-2-((S)-2,2-dimethyl-6-methylene-cyclohexylmethyl)-4-methoxy-phenoxy]-tert-butyl-dimethyl-silane

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 18h; Ambient temperature;
DOI:10.1021/jm950747d

Reference yield:

: 156170-20-6
[5-Bromo-2-((1R,3R)-3-bromo-2,2-dimethyl-6-methylene-cyclohexylmethyl)-4-methoxy-phenoxy]-tert-butyl-dimethyl-silane

: 5-Bromo-2-((1S,5R)-5-hydroxy-2,2-dimethyl-6-methylene-cyclohexylmethyl)-4-methoxy-phenol

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / AIBN, n-Bu₃SnH / benzene / 18 h / Ambient temperature

2: SeO₂, t-BuOOH / CH₂Cl₂

3: t-Bu₄NF / tetrahydrofuran / Ambient temperature

With tert.-butylhydroperoxide; selenium(IV) oxide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; tetra(tert-butyl)-ammonium fluoride; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/jm950747d