ethyl 2,2-bis(4-dimethylaminophenyl)-9-methoxy-2H-naphtho[1,2-b]pyran-5-carboxylate

Base Information

Chemical Name:ethyl 2,2-bis(4-dimethylaminophenyl)-9-methoxy-2H-naphtho[1,2-b]pyran-5-carboxylate
CAS No.:1259944-64-3
Molecular Formula:C₃₃H₃₄N₂O₄
Molecular Weight:522.644
Hs Code.:

Synonyms:ethyl 2,2-bis(4-dimethylaminophenyl)-9-methoxy-2H-naphtho[1,2-b]pyran-5-carboxylate

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Chemical Property of ethyl 2,2-bis(4-dimethylaminophenyl)-9-methoxy-2H-naphtho[1,2-b]pyran-5-carboxylate

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Technology Process of ethyl 2,2-bis(4-dimethylaminophenyl)-9-methoxy-2H-naphtho[1,2-b]pyran-5-carboxylate

There total 1 articles about ethyl 2,2-bis(4-dimethylaminophenyl)-9-methoxy-2H-naphtho[1,2-b]pyran-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.5%

: 102164-16-9
1,1-di[4,4'-bis(dimethylamino)phenyl]-2-propyn-1-ol

: 538343-03-2
ethyl 4-hydroxy-6-methoxynaphthalene-2-carboxylate

: 1259944-64-3
ethyl 2,2-bis(4-dimethylaminophenyl)-9-methoxy-2H-naphtho[1,2-b]pyran-5-carboxylate

Guidance literature:: With Sasol Pural MG-30; In toluene; Reflux;
DOI:10.1039/c0cc02986f

Reference yield: 59.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 1259944-64-3
ethyl 2,2-bis(4-dimethylaminophenyl)-9-methoxy-2H-naphtho[1,2-b]pyran-5-carboxylate

: 1259944-69-8
2,2-bis(4-dimethylaminophenyl)-9-methoxy-5-[1,1-bis(4-methoxyphenyl)-1-hydroxymethyl]-2H-naphtho[1,2-b]pyran

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -70 - 20 ℃; Inert atmosphere;
DOI:10.1039/c0cc02986f

Reference yield:

: 1259944-64-3
ethyl 2,2-bis(4-dimethylaminophenyl)-9-methoxy-2H-naphtho[1,2-b]pyran-5-carboxylate

: CH₃O₃S^(1-)*C₄₅H₄₃N₂O₄⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane; cyclohexane / 2 h / -70 °C / Inert atmosphere

1.2: -70 - 20 °C / Inert atmosphere

2.1: dichloromethane

With n-butyllithium; In tetrahydrofuran; hexane; dichloromethane; cyclohexane;
DOI:10.1016/j.dyepig.2011.07.004