Methyl (3S)-3-{N-benzyl-N-[(S)-1-phenylethyl]amino}-6-benzyloxyhexanoate

Base Information

• Chemical Name: Methyl (3S)-3-{N-benzyl-N-[(S)-1-phenylethyl]amino}-6-benzyloxyhexanoate
• CAS No.: 219700-38-6
• Molecular Formula: C₂₉H₃₅NO₃
• Molecular Weight: 445.602

Synonyms:Methyl (3S)-3-{N-benzyl-N-[(S)-1-phenylethyl]amino}-6-benzyloxyhexanoate

Chemical Property of Methyl (3S)-3-{N-benzyl-N-[(S)-1-phenylethyl]amino}-6-benzyloxyhexanoate

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Technology Process of Methyl (3S)-3-{N-benzyl-N-[(S)-1-phenylethyl]amino}-6-benzyloxyhexanoate

There total 9 articles about Methyl (3S)-3-{N-benzyl-N-[(S)-1-phenylethyl]amino}-6-benzyloxyhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

6-benzyloxy-2(E)-hexenoic acid methyl ester (91020-91-6) + lithium N-benzyl-N-((S)-1-phenylethyl)amide → Methyl (3S)-3-{N-benzyl-N-[(S)-1-phenylethyl]amino}-6-benzyloxyhexanoate (219700-38-6)

Guidance literature:

DOI:10.1016/S0040-4039(98)02076-0

Reference yield: 81.0%

(S)-N-benzyl-1-phenylethylamine (17480-69-2) + 6-benzyloxy-2(E)-hexenoic acid methyl ester (91020-91-6) → Methyl (3S)-3-{N-benzyl-N-[(S)-1-phenylethyl]amino}-6-benzyloxyhexanoate (219700-38-6)

Guidance literature:

(S)-N-benzyl-1-phenylethylamine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.75h;

6-benzyloxy-2(E)-hexenoic acid methyl ester; at -78 ℃; for 1h;

Reference yield: 30.0%

2-(pent-1-yn-1-yl)aniline (26059-38-1) + thiophenol (108-98-5) → 2-propyl-indole (13228-41-6) + Methyl (3S)-3-{N-benzyl-N-[(S)-1-phenylethyl]amino}-6-benzyloxyhexanoate (219700-38-6) + (2S,3R)-3-{(S)-4-Benzyloxy-1-[benzyl-((S)-1-phenyl-ethyl)-amino]-butyl}-2-hydroxy-2-methyl-succinic acid dimethyl ester (219700-40-0) + (2R,3R)-3-{(S)-4-Benzyloxy-1-[benzyl-((S)-1-phenyl-ethyl)-amino]-butyl}-2-hydroxy-2-methyl-succinic acid dimethyl ester (219700-39-7)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In various solvent(s); at 150 ℃; for 1h;

DOI:10.1016/S0040-4039(98)01998-4

upstream raw materials:

6-benzyloxy-2(E)-hexenoic acid methyl ester

2-(pent-1-yn-1-yl)aniline

thiophenol

(S)-N-benzyl-1-phenylethylamine

Downstream raw materials:

(2S,3R)-3-{(S)-4-Benzyloxy-1-[benzyl-((S)-1-phenyl-ethyl)-amino]-butyl}-2-hydroxy-2-methyl-succinic acid dimethyl ester

(2R,3R)-3-{(S)-4-Benzyloxy-1-[benzyl-((S)-1-phenyl-ethyl)-amino]-butyl}-2-hydroxy-2-methyl-succinic acid dimethyl ester

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