N-[2-(2-bromo-5-hydroxy-4-methoxyphenyl)-ethyl]-N-[(4-hydroxyphenyl)methyl]-formamide

Base Information

Chemical Name:N-[2-(2-bromo-5-hydroxy-4-methoxyphenyl)-ethyl]-N-[(4-hydroxyphenyl)methyl]-formamide
CAS No.:365571-98-8
Molecular Formula:C₁₇H₁₈BrNO₄
Molecular Weight:380.238
Hs Code.:

Synonyms:N-[2-(2-bromo-5-hydroxy-4-methoxyphenyl)-ethyl]-N-[(4-hydroxyphenyl)methyl]-formamide

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Chemical Property of N-[2-(2-bromo-5-hydroxy-4-methoxyphenyl)-ethyl]-N-[(4-hydroxyphenyl)methyl]-formamide

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Technology Process of N-[2-(2-bromo-5-hydroxy-4-methoxyphenyl)-ethyl]-N-[(4-hydroxyphenyl)methyl]-formamide

There total 10 articles about N-[2-(2-bromo-5-hydroxy-4-methoxyphenyl)-ethyl]-N-[(4-hydroxyphenyl)methyl]-formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 109-94-4
formic acid ethyl ester

: 365571-97-7
4-bromo-5-[N-[(4-hydroxyphenyl)methyl]-2-aminoethyl]-2-methoxyphenol

: 365571-98-8
N-[2-(2-bromo-5-hydroxy-4-methoxyphenyl)-ethyl]-N-[(4-hydroxyphenyl)methyl]-formamide

Guidance literature:: With dmap; formic acid; In 1,4-dioxane; N,N-dimethyl-formamide; for 24h; Heating;
DOI:10.1016/S0040-4020(01)01235-2

Reference yield:

: 4-Bromo-2-methoxy-5-((Z)-2-methoxy-vinyl)-phenol

: 365571-98-8
N-[2-(2-bromo-5-hydroxy-4-methoxyphenyl)-ethyl]-N-[(4-hydroxyphenyl)methyl]-formamide

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / 2N HCl / tetrahydrofuran / 2.5 h / Heating

2: 35 percent / zinc dust; 2N HCl / tetrahydrofuran / 5 h / Heating

3: 72 percent / 4-(dimethylamino)pyridine; formic acid / dioxane; dimethylformamide / 24 h / Heating

With hydrogenchloride; dmap; formic acid; zinc; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)01235-2

Reference yield:

: 444575-77-3
2-bromo-5-hydroxy-4-methoxybenzeneacetaldehyde

: 365571-98-8
N-[2-(2-bromo-5-hydroxy-4-methoxyphenyl)-ethyl]-N-[(4-hydroxyphenyl)methyl]-formamide

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / zinc dust; 2N HCl / tetrahydrofuran / 5 h / Heating

2: 72 percent / 4-(dimethylamino)pyridine; formic acid / dioxane; dimethylformamide / 24 h / Heating

With hydrogenchloride; dmap; formic acid; zinc; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)01235-2