(2S,3S)-2-BENZYLOXY-3,4-O-ISOPROPYLIDENE-BUTAN-1-OL

Base Information

Chemical Name:(2S,3S)-2-BENZYLOXY-3,4-O-ISOPROPYLIDENE-BUTAN-1-OL
CAS No.:104322-67-0
Molecular Formula:C14H20 O4
Molecular Weight:252.31
Hs Code.:2932999099
Mol file:104322-67-0.mol

Synonyms:1,3-Dioxolane-4-ethanol,2,2-dimethyl-b-(phenylmethoxy)-,[S-(R*,S*)]-

Suppliers and Price of (2S,3S)-2-BENZYLOXY-3,4-O-ISOPROPYLIDENE-BUTAN-1-OL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(2S,3S)-2-BENZYLOXY-3,4-ORTHO-ISOPROPYLIDENE-BUTAN-1-OL 98.00%
100G
$ 3422.27

Total 2 raw suppliers

Chemical Property of (2S,3S)-2-BENZYLOXY-3,4-O-ISOPROPYLIDENE-BUTAN-1-OL

Chemical Property:

Vapor Pressure:2.49E-06mmHg at 25°C
Refractive Index:1.513
Boiling Point:376.2°Cat760mmHg
Flash Point:181.3°C
PSA：47.92000
Density:1.116g/cm³
LogP:1.71560

Purity/Quality:: (2S,3S)-2-BENZYLOXY-3,4-ORTHO-ISOPROPYLIDENE-BUTAN-1-OL 98.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2S,3S)-2-BENZYLOXY-3,4-O-ISOPROPYLIDENE-BUTAN-1-OL

There total 14 articles about (2S,3S)-2-BENZYLOXY-3,4-O-ISOPROPYLIDENE-BUTAN-1-OL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 340699-15-2
ethyl (2S,3S)-2-O-benzyl-3,4-O-isopropylidene-2,3,4-trihydroxybutanoate

: 104322-67-0
(R)-2-Benzyloxy-2-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethanol

Guidance literature:: With lithium borohydride; In methanol; diethyl ether; at 0 ℃; for 2h;
DOI:10.1021/jo0521192

Reference yield: 80.0%

: 84379-51-1,84379-52-2,124909-02-0,127000-44-6
dl-2-O-benzylerythritol

: 77-76-9
2,2-dimethoxy-propane

: 84379-53-3,84379-54-4,104322-67-0,111462-38-5,116365-24-3,116405-02-8
dl-2-O-benzyl-3,4-O-isopropylideneerythritol

Guidance literature:: toluene-4-sulfonic acid; In benzene; for 3h; Heating;
DOI:10.1248/cpb.37.2379

Reference yield:

: 100-52-7
benzaldehyde

: 84379-53-3,84379-54-4,104322-67-0,111462-38-5,116365-24-3,116405-02-8
dl-2-O-benzyl-3,4-O-isopropylideneerythritol

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / p-TsOH (H₂O) / toluene / 8 h / Heating

2: 65 percent / LiAlH₄-AlCl₃ / diethyl ether; CH₂Cl₂ / 3 h / Ambient temperature

3: 80 percent / p-TsOH (H₂O) / benzene / 3 h / Heating

With lithium aluminium tetrahydride; aluminium trichloride; toluene-4-sulfonic acid; toluene-4-sulfonic acid; In diethyl ether; dichloromethane; toluene; benzene;
DOI:10.1248/cpb.37.2379