mesityl-lead triacetate

Base Information

Chemical Name:mesityl-lead triacetate
CAS No.:128796-44-1
Molecular Formula:C₁₅H₂₀O₆Pb
Molecular Weight:503.52
Hs Code.:

Synonyms:mesityl-lead triacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of mesityl-lead triacetate

Chemical Property:

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Technology Process of mesityl-lead triacetate

There total 3 articles about mesityl-lead triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: lead(IV) tetraacetate

: 26562-17-4
{2,4,6-(CH3)3C6H2}2Hg

: 128796-44-1
C₆H₂(CH₃)3Pb(OOCCH₃)3

Guidance literature:: In toluene; addn. of Pb(OAc)4 in toluene to a soln. of Hg-compd. in toluene, stirring at room temp. for 3 days (orange to brown soln.); shaking out the soln. with ethyleneglycol (pale yellow soln.), drying (Na2SO4), filtration, evapn. of filtrate (vac., 50°C), dissoln. of residue in abs. CHCl3, fractional crystn. with petroleum ether (40-60°C) at -30°C; elem. anal.;
DOI:10.1016/0022-328X(92)83382-R

Reference yield: 44.0%

: 546-67-8
lead(IV) tetraacetate

: 5806-59-7
mesityllithium

: 128796-44-1
mesityl-lead triacetate

Guidance literature:: mercury(II) diacetate; In chloroform; addn. of B-compd. to stirred mixt. of Pb-compd. and Hg-compd. in CHCl3 over 15 min (40°C), stirring (40°C, 1 h and room temp. overnight); filtration (Celite), concn. (40°C), addn. of petroleum ether, standing (0°C, overnight), stirring in mixt. of acetic acid and CHCl3, washing (H2O), drying (Na2SO4), concn., addn. of petroleum ether, crystn. (0°C); elem. anal.;

Reference yield:

: 5980-97-2
mesitylboronic acid

: 546-67-8
lead(IV) tetraacetate

: 128796-44-1
mesityl-lead triacetate

Guidance literature:: mesitylboronic acid; lead(IV) tetraacetate; With mercury(II) diacetate; In chloroform; at 20 - 40 ℃; for 4.25h; Inert atmosphere;

With potassium carbonate; In chloroform; at 20 ℃; for 0.166667h; Inert atmosphere;