[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]dichlorostibine

Base Information

Chemical Name:[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]dichlorostibine
CAS No.:201533-94-0
Molecular Formula:C₂₇H₅₉Cl₂SbSi₆
Molecular Weight:744.934
Hs Code.:

Synonyms:[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]dichlorostibine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]dichlorostibine

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Technology Process of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]dichlorostibine

There total 1 articles about [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]dichlorostibine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 10025-91-9
antimony(III) chloride

: 115160-05-9
1-bromo-2,4,6-tris[bis(trimethylsilyl)methyl]benzene

: 201533-94-0
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]dichlorostibine

Guidance literature:: With tert-butyl lithium; In tetrahydrofuran; byproducts: LiBr; a soln. of phenylbromide in THF was treated with tert-butyl lithium at -78°C, after 30 min a soln. of SbCl3 was added, the mixt. was warmed to room temp. and stirred for 2 h (Ar); evapd., hexane was added, filtered, the solvent was removed, pptd. from CH2Cl2-isopropanol; elem. anal.;
DOI:10.1246/bcsj.75.661