(4-ISOPROPOXY-PHENYL)-HYDRAZINE HYDROCHLORIDE

Base Information

• Chemical Name: (4-ISOPROPOXY-PHENYL)-HYDRAZINE HYDROCHLORIDE
• CAS No.: 104033-62-7
• Molecular Formula: C9H14 N2 O . Cl H
• Molecular Weight: 202.684
• Mol file: 104033-62-7.mol

Synonyms:Hydrazine,[4-(1-methylethoxy)phenyl]-, monohydrochloride (9CI)

Chemical Property of (4-ISOPROPOXY-PHENYL)-HYDRAZINE HYDROCHLORIDE

Chemical Property:

• Vapor Pressure: 0.00144mmHg at 25°C
• Refractive Index: 1.574
• Boiling Point: 296.4°C at 760 mmHg
• Flash Point: 133.1°C
• PSA: 26.02000
• Density: 1.083g/cm³
• LogP: 3.04130
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

(4-Isopropoxyphenyl)hydrazinehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: (4-Isopropoxyphenyl)hydrazine Hydrochloride can be used as light-sensitive copying material.

Technology Process of (4-ISOPROPOXY-PHENYL)-HYDRAZINE HYDROCHLORIDE

There total 3 articles about (4-ISOPROPOXY-PHENYL)-HYDRAZINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4-(isopropoxy)aniline (7664-66-6) → (4-isopropoxyphenyl)hydrazine hydrochloride (104033-62-7)

Guidance literature:

4-(isopropoxy)aniline; With hydrogenchloride; In water; at 0 - 20 ℃; for 0.416667h; Inert atmosphere;

With sodium nitrite; In water; Inert atmosphere; Cooling;

With tin(II) chloride dihdyrate; Inert atmosphere;

DOI:10.1002/cmdc.202000278

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → (4-isopropoxyphenyl)hydrazine hydrochloride (104033-62-7)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 - 60 °C / Inert atmosphere

2.1: tin(II) chloride dihdyrate / ethyl acetate / 18 h / 50 °C

3.1: hydrogenchloride / water / 0.42 h / 0 - 20 °C / Inert atmosphere

3.2: Inert atmosphere; Cooling

3.3: Inert atmosphere

With hydrogenchloride; tin(II) chloride dihdyrate; potassium carbonate; In water; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1002/cmdc.202000278

Reference yield:

1-isopropoxy-4-nitrobenzene (26455-31-2) → (4-isopropoxyphenyl)hydrazine hydrochloride (104033-62-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: tin(II) chloride dihdyrate / ethyl acetate / 18 h / 50 °C

2.1: hydrogenchloride / water / 0.42 h / 0 - 20 °C / Inert atmosphere

2.2: Inert atmosphere; Cooling

2.3: Inert atmosphere

With hydrogenchloride; tin(II) chloride dihdyrate; In water; ethyl acetate;

DOI:10.1002/cmdc.202000278

upstream raw materials:

4-(isopropoxy)aniline

4-nitro-phenol

1-isopropoxy-4-nitrobenzene

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