1H-Imidazole, 4-ethenyl-1-(phenylmethyl)-

Base Information

Chemical Name:1H-Imidazole, 4-ethenyl-1-(phenylmethyl)-
CAS No.:86803-30-7
Molecular Formula:C₁₂H₁₂N₂
Molecular Weight:184.241
Hs Code.:
DSSTox Substance ID:DTXSID801279965
Nikkaji Number:J1.844.749E

Synonyms:86803-30-7;1H-Imidazole, 4-ethenyl-1-(phenylmethyl)-;DTXSID801279965;4-Ethenyl-1-(phenylmethyl)-1H-imidazole

Suppliers and Price of 1H-Imidazole, 4-ethenyl-1-(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Imidazole, 4-ethenyl-1-(phenylmethyl)-

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:184.100048391
Heavy Atom Count:14
Complexity:185

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CC1=CN(C=N1)CC2=CC=CC=C2

Technology Process of 1H-Imidazole, 4-ethenyl-1-(phenylmethyl)-

There total 6 articles about 1H-Imidazole, 4-ethenyl-1-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 7486-35-3
tri-n-butyl(vinyl)tin

: 536760-32-4
1-benzyl-4-iodo-1H-imidazole

: 86803-30-7
1-benzyl-4-ethenyl-1H-imidazole

Guidance literature:: With triphenylphosphine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In N,N-dimethyl-formamide; at 90 ℃;
DOI:10.3987/com-02-9598

Reference yield: 70.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 85102-93-8
1-benzyl-4-imidazolecarboxaldehyde

: 86803-30-7
1-benzyl-4-ethenyl-1H-imidazole

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 65 ℃; for 3h;
DOI:10.1021/jo00168a062

Reference yield:

: 100-44-7
benzyl chloride

: 86803-30-7
1-benzyl-4-ethenyl-1H-imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NaOH / H₂O; dimethylformamide / 1 h / 30 - 40 °C

2: 90 percent / Pd₂(dba)3; PPh₃ / dimethylformamide / 22 h / 90 °C

With sodium hydroxide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; triphenylphosphine; In water; N,N-dimethyl-formamide; 2: Stille cross-coupling;
DOI:10.1021/jo0626008