Cu(II)(1,3-bis(2-pyridylimino)isoindolinate)(O-benzoylsalicylic acid)

Base Information

• Chemical Name: Cu(II)(1,3-bis(2-pyridylimino)isoindolinate)(O-benzoylsalicylic acid)
• CAS No.: 300662-53-7
• Molecular Formula: C₃₂H₂₁CuN₅O₄
• Molecular Weight: 603.096
• Mol file: 300662-53-7.mol

Synonyms:Cu(II)(1,3-bis(2-pyridylimino)isoindolinate)(O-benzoylsalicylic acid)

Chemical Property of Cu(II)(1,3-bis(2-pyridylimino)isoindolinate)(O-benzoylsalicylic acid)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cu(II)(1,3-bis(2-pyridylimino)isoindolinate)(O-benzoylsalicylic acid)

There total 4 articles about Cu(II)(1,3-bis(2-pyridylimino)isoindolinate)(O-benzoylsalicylic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

o-benzoyloxybenzoic acid (4578-66-9) + 1,3-bis-(2-pyridylimino)isoindoline (14526-01-3) + mesitylcopper(I) (75732-01-3) → Cu(II)(1,3-bis(2-pyridylimino)isoindolinate)(O-benzoylsalicylic acid) (300662-53-7)

Guidance literature:

With O₂; In acetonitrile; mesitylcopper(I), O-benzoylsalicylic acid, and the isoindoline were dissolved in acetonitrile and stirred under O2 atm. for 3 h; ppt. was filtered off, washed with ether, and dried under vac.; elem. anal.;

DOI:10.1021/ic990521r

Reference yield: 65.0%

(Cu(II)(flavonolate)(1,3-bis(2-pyridylimino)isoindolinate)) (300662-51-5) → Cu(II)(1,3-bis(2-pyridylimino)isoindolinate)(O-benzoylsalicylic acid) (300662-53-7)

Guidance literature:

With O₂; In acetonitrile; Cu(II)(fla)(ind) in acetonitrile was treated with O2 at 80°C for30 h; ppt. was filtered off, washed with acetonitrile and dried under vac.;

DOI:10.1021/ic990521r

Reference yield: 50.0%

(Cu(I)(flavonolate)(1,3-bis(2-pyridylimino)isoindoline)) (300662-50-4) → Cu(II)(1,3-bis(2-pyridylimino)isoindolinate)(O-benzoylsalicylic acid) (300662-53-7)

Guidance literature:

With O₂; In acetonitrile; Cu(I)(fla)(indH) in acetonitrile was treated with O2 at 80°C for25 h; ppt. was filtered off, washed with acetonitrile and dried under vac.;

DOI:10.1021/ic990521r

upstream raw materials:

o-benzoyloxybenzoic acid

1,3-bis-(2-pyridylimino)isoindoline

mesitylcopper(I)

(Cu(I)(flavonolate)(1,3-bis(2-pyridylimino)isoindoline))