(E)-N-(5-chloro-2-{3-[3-(4-fluorobenzyl)-3,8-diazabicyclo[3.2.1]oct-8-yl]-3-oxopropenyl}-phenyl)-N'-cyanoguanidine

Base Information

Chemical Name:(E)-N-(5-chloro-2-{3-[3-(4-fluorobenzyl)-3,8-diazabicyclo[3.2.1]oct-8-yl]-3-oxopropenyl}-phenyl)-N'-cyanoguanidine
CAS No.:868406-33-1
Molecular Formula:C₂₄H₂₄ClFN₆O
Molecular Weight:466.946
Hs Code.:

Synonyms:(E)-N-(5-chloro-2-{3-[3-(4-fluorobenzyl)-3,8-diazabicyclo[3.2.1]oct-8-yl]-3-oxopropenyl}-phenyl)-N'-cyanoguanidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(5-chloro-2-{3-[3-(4-fluorobenzyl)-3,8-diazabicyclo[3.2.1]oct-8-yl]-3-oxopropenyl}-phenyl)-N'-cyanoguanidine

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Technology Process of (E)-N-(5-chloro-2-{3-[3-(4-fluorobenzyl)-3,8-diazabicyclo[3.2.1]oct-8-yl]-3-oxopropenyl}-phenyl)-N'-cyanoguanidine

There total 2 articles about (E)-N-(5-chloro-2-{3-[3-(4-fluorobenzyl)-3,8-diazabicyclo[3.2.1]oct-8-yl]-3-oxopropenyl}-phenyl)-N'-cyanoguanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 868406-32-0
(E)-3-(2-amino-4-chlorophenyl)-1-[3-(4-fluorobenzyl)-3,8-diazabicyclo[3.2.1]oct-8-yl]-propenone

: 1934-75-4
sodium dicyanamide

: 868406-33-1
(E)-N-(5-chloro-2-{3-[3-(4-fluorobenzyl)-3,8-diazabicyclo[3.2.1]oct-8-yl]-3-oxopropenyl}-phenyl)-N'-cyanoguanidine

Guidance literature:: With hydrogenchloride; In 2-ethoxy-ethanol; water; for 0.166667h; Heating / reflux;

Reference yield:

: 868406-30-8
(E)-(5-chloro-2-{3-[3-(4-fluorobenzyl)-3,8-diazabicyclo[3.2.1]oct-8-yl]-3-oxopropenyl}phenyl)-carbamic acid tert-butyl ester

: 868406-33-1
(E)-N-(5-chloro-2-{3-[3-(4-fluorobenzyl)-3,8-diazabicyclo[3.2.1]oct-8-yl]-3-oxopropenyl}-phenyl)-N'-cyanoguanidine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; ethanol; water / 0.03 h

2: hydrogenchloride / 2-ethoxy-ethanol; water / 0.17 h / Heating / reflux

With hydrogenchloride; ethanol; water; In 2-ethoxy-ethanol; water;