CID 53249392

Base Information

• Chemical Name: CID 53249392
• CAS No.: 1934-75-4
• Molecular Formula: C2HN3. Na
• Molecular Weight: 89.0319
• Hs Code.: 29269090
• Mol file: 1934-75-4.mol

Synonyms:AKOS015853632;AKOS028109540

Chemical Property of CID 53249392

Chemical Property:

• Appearance/Colour: White to off-white powder
• Melting Point: 300 °C
• Boiling Point: 41.5 °C at 760 mmHg
• Flash Point: 8.5 °C
• PSA: 50.82000
• LogP: -0.28514
• Storage Temp.: Inert atmosphere,Room Temperature
• Sensitive.: Hygroscopic
• Solubility.: Methanol (sparingly), Water
• Water Solubility.: 260 g/L (30 ºC)
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 90.00681633
• Heavy Atom Count: 6
• Complexity: 82.6

Purity/Quality:

98% ^*data from raw suppliers

N-CyanocyanamideSodiumSalt ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi, Xn
• Hazard Codes: Xn,Xi
• Statements: 22-36/37/38
• Safety Statements: 26-36-37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C(#N)NC#N.[Na]
• Uses: Sodium dicyanamide is used or the production of pharmaceuticals (e.g. chlorhexidine, biguanide, proguanil and alexidine). Product Data Sheet Reactant for preparation of:Nickel diacetylpyridine dioximate pentanuclear, octanuclear and decanuclear cluster complexesDecanuclear manganese(II/III) oxo azide diolate clusters as supertetrahedral building-blocks to design extended magnetic networksRuthenium bipyridine complexes entrapped in iron and manganese dicyanamide two-dimensional anionic sheet-like coordination polymeric networks exhibiting dual emission photoluminescenceLead dicyanamide-bridged nitronyl nitroxide radical polymeric complexAntiferromagnetically coupled hexanuclear copper(II) Schiff base complexes with dicyanamido bridgesCuII2L based polymeric ladders using dicyanamide bridgesLuminous hexacoordinated coordination polymers of cadmium(II), containing dicyanamide bridges

Technology Process of CID 53249392

There total 30 articles about CID 53249392 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

CYANAMID (420-04-2) + cyanogen chloride (506-77-4) → sodium N-cyanoisourea (76989-89-4) + sodium dicyanamide (1934-75-4) + sodium chloride (7647-14-5)

Guidance literature:

With sodium hydroxide; In water; at 70 - 75 ℃; under 1050.11 Torr; pH=7.2 - 8.0; Purification / work up;

Reference yield: 87.0%

CYANAMID (420-04-2) + cyanogen chloride (506-77-4) → sodium dicyanamide (1934-75-4)

Guidance literature:

With sodium hydroxide; In water; at 50 - 55 ℃; under 1050.11 Torr; pH=7.2 - 8.0;

Reference yield: 72.0%

bromocyane (506-68-3) + CYANAMID (420-04-2) → sodium dicyanamide (1934-75-4)

Guidance literature:

CYANAMID; With sodium; In ethanol; at 20 ℃; for 1.5h;

bromocyane; In ethanol; for 2.5h;

DOI:10.1021/acs.analchem.0c04464

upstream raw materials:

bromocyane

sodium cyanamide

CYANAMID

cyanogen chloride

Downstream raw materials:

N-benzyl-N'-cyano-N-methyl-guanidine

N¹,N¹-Di-p-tolyl-cyanguanidin

N''-cyano-N-(2-methoxyphenyl)guanidine

N''-cyano-N-(2-chlorophenyl)guanidine

Refernces

• 1、 Singh, Virendra V.,Kumar, Vinod,Biswas, Utpal,Boopathi, Mannan,Ganesan, Kumaran,Gupta, Arvind K.. "Luminol-Based Turn-On Fluorescent Sensor for Selective and Sensitive Detection of Sulfur Mustard at Ambient Temperature". . p. 1193 - 1199. Retrieved 2021.