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1934-75-4

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1934-75-4 Usage

Chemical Properties

White to off-white powder

Uses

Different sources of media describe the Uses of 1934-75-4 differently. You can refer to the following data:
1. Sodium dicyanamide is used or the production of pharmaceuticals (e.g. chlorhexidine, biguanide, proguanil and alexidine). Product Data Sheet
2. Reactant for preparation of:Nickel diacetylpyridine dioximate pentanuclear, octanuclear and decanuclear cluster complexesDecanuclear manganese(II/III) oxo azide diolate clusters as supertetrahedral building-blocks to design extended magnetic networksRuthenium bipyridine complexes entrapped in iron and manganese dicyanamide two-dimensional anionic sheet-like coordination polymeric networks exhibiting dual emission photoluminescenceLead dicyanamide-bridged nitronyl nitroxide radical polymeric complexAntiferromagnetically coupled hexanuclear copper(II) Schiff base complexes with dicyanamido bridgesCuII2L based polymeric ladders using dicyanamide bridgesLuminous hexacoordinated coordination polymers of cadmium(II), containing dicyanamide bridges

Check Digit Verification of cas no

The CAS Registry Mumber 1934-75-4 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 1,9,3 and 4 respectively; the second part has 2 digits, 7 and 5 respectively.
Calculate Digit Verification of CAS Registry Number 1934-75:
(6*1)+(5*9)+(4*3)+(3*4)+(2*7)+(1*5)=94
94 % 10 = 4
So 1934-75-4 is a valid CAS Registry Number.
InChI:InChI=1/C2N3.Na/c3-1-5-2-4;/q-1;+1/rC2N3Na/c3-1-5(6)2-4

1934-75-4 Well-known Company Product Price

  • Brand
  • (Code)Product description
  • CAS number
  • Packaging
  • Price
  • Detail
  • Alfa Aesar

  • (B21634)  Sodium dicyanamide, 96%   

  • 1934-75-4

  • 25g

  • 589.0CNY

  • Detail
  • Alfa Aesar

  • (B21634)  Sodium dicyanamide, 96%   

  • 1934-75-4

  • 100g

  • 1492.0CNY

  • Detail
  • Alfa Aesar

  • (B21634)  Sodium dicyanamide, 96%   

  • 1934-75-4

  • 500g

  • 3421.0CNY

  • Detail
  • Aldrich

  • (178322)  Sodiumdicyanamide  96%

  • 1934-75-4

  • 178322-25G

  • 382.59CNY

  • Detail
  • Aldrich

  • (178322)  Sodiumdicyanamide  96%

  • 1934-75-4

  • 178322-100G

  • 1,028.43CNY

  • Detail

1934-75-4SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 11, 2017

Revision Date: Aug 11, 2017

1.Identification

1.1 GHS Product identifier

Product name sodium,dicyanoazanide

1.2 Other means of identification

Product number -
Other names Dicyanamide,sodium salt

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:1934-75-4 SDS

1934-75-4Synthetic route

CYANAMID
420-04-2

CYANAMID

cyanogen chloride
506-77-4

cyanogen chloride

A

sodium N-cyanoisourea
76989-89-4

sodium N-cyanoisourea

B

sodium dicyanamide
1934-75-4

sodium dicyanamide

C

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
With sodium hydroxide In water at 70 - 75℃; under 1050.11 Torr; pH=7.2 - 8.0; Purification / work up;A n/a
B 94%
C n/a
CYANAMID
420-04-2

CYANAMID

cyanogen chloride
506-77-4

cyanogen chloride

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
With sodium hydroxide In water at 50 - 55℃; under 1050.11 Torr; pH=7.2 - 8.0;87%
With sodium hydroxide In water at 70 - 75℃; under 1050.11 Torr; pH=7.2 - 8.0; Product distribution / selectivity;83%
With sodium hydroxide In water at 70 - 75℃; under 1050.11 Torr; pH=7.2 - 8.0; Product distribution / selectivity;82%
With sodium hydroxide In water at 50 - 55℃; under 1050.11 Torr; pH=7.2 - 8.0; Product distribution / selectivity;79%
With sodium hydroxide In water at 70 - 75℃; for 1.58333h; pH=7.5 - 8.0;76%
bromocyane
506-68-3

bromocyane

CYANAMID
420-04-2

CYANAMID

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
Stage #1: CYANAMID With sodium In ethanol at 20℃; for 1.5h;
Stage #2: bromocyane In ethanol for 2.5h;
72%
bromocyane
506-68-3

bromocyane

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
With water
bromocyane
506-68-3

bromocyane

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
With sodium amide in der Kugelmuehle;
sodium salt of O-ethyl-N-cyano-isourea

sodium salt of O-ethyl-N-cyano-isourea

sodium dicyanamide
1934-75-4

sodium dicyanamide

cyanogen chloride
506-77-4

cyanogen chloride

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
With sodium amide In not given byproducts: NH3, NaCl; at room temp., in ball mill;
sodium amide

sodium amide

cyanogen chloride
506-77-4

cyanogen chloride

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
byproducts: NH3, NaCl; in ball mill; reactn. complete after 60 h at room temp.;
byproducts: NH3, NaCl; in ball mill; reactn. complete after 60 h at room temp.;
sodium amide

sodium amide

cyanogen chloride
506-77-4

cyanogen chloride

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In neat (no solvent) constantly grinding in ball mill at ambient temp., 60h; complete exclusion of air;;
In neat (no solvent) constantly grinding in ball mill at ambient temp., 60h; complete exclusion of air;;
disodium cyanamide
20611-81-8

disodium cyanamide

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
With NCBr In neat (no solvent) grinding in ball mill;;
With NCBr In neat (no solvent) grinding in ball mill;;
bromocyane
506-68-3

bromocyane

disodium cyanamide
20611-81-8

disodium cyanamide

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In water addn. of aq. Na2NCN soln. to CNBr with cooling up to neutral soln.; evapn. on the water-bath;; recrystn. from ethanol;;
copper(II) dicyanamide
14890-16-5, 18447-47-7, 21962-69-6

copper(II) dicyanamide

sodium phosphate

sodium phosphate

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
dicyanamide; calcium-bis-(dicyano-amide)
14723-18-3

dicyanamide; calcium-bis-(dicyano-amide)

sodium phosphate

sodium phosphate

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
zinc dicyanamide

zinc dicyanamide

sodium phosphate

sodium phosphate

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
bromocyane
506-68-3

bromocyane

sodium amide

sodium amide

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
byproducts: NH3, NaBr; in ball mill; reactn. complete after 60 h at room temp.;
byproducts: NH3, NaBr; in ball mill; reactn. complete after 60 h at room temp.;
bromocyane
506-68-3

bromocyane

CYANAMID
420-04-2

CYANAMID

A

{NHC(NHCN)(OC2H5)}(1-)*Na(1+)={NHC(NHCN)(OC2H5)}Na

{NHC(NHCN)(OC2H5)}(1-)*Na(1+)={NHC(NHCN)(OC2H5)}Na

B

sodium dicyanamide
1934-75-4

sodium dicyanamide

C

sodium bromide
7647-15-6

sodium bromide

Conditions
ConditionsYield
With Na-alcoholate In ethanol
With Na-alcoholate In ethanol
sodium amide

sodium amide

bromocyane
506-68-3

bromocyane

A

ammonia
7664-41-7

ammonia

B

sodium dicyanamide
1934-75-4

sodium dicyanamide

C

sodium bromide
7647-15-6

sodium bromide

sodium amide

sodium amide

bromocyane
506-68-3

bromocyane

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In neat (no solvent) constantly grinding in ball mill at ambient temp., 60h; complete exclusion of air;;
In neat (no solvent) constantly grinding in ball mill at ambient temp., 60h; complete exclusion of air;;
cyanogen iodide
506-78-5

cyanogen iodide

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
With sodium amide In neat (no solvent) byproducts: NH3, NaI; at room temp., in ball mill, extn. with water;
cyanogen iodide
506-78-5

cyanogen iodide

sodium amide

sodium amide

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
byproducts: NH3, NaI; in ball mill; reactn. complete after 60 h at room temp.;
byproducts: NH3, NaI; in ball mill; reactn. complete after 60 h at room temp.;
sodium amide

sodium amide

cyanogen iodide
506-78-5

cyanogen iodide

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In neat (no solvent) constantly grinding in ball mill at ambient temp., 60h; complete exclusion of air;;
In neat (no solvent) constantly grinding in ball mill at ambient temp., 60h; complete exclusion of air;;
sodium sulfide

sodium sulfide

silver dicyanamide
51342-29-1

silver dicyanamide

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In water crystn. from hot MeOH;
copper(II) dicyanamide
14890-16-5, 18447-47-7, 21962-69-6

copper(II) dicyanamide

sodium hydroxide
1310-73-2

sodium hydroxide

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
dicyanamide; calcium-bis-(dicyano-amide)
14723-18-3

dicyanamide; calcium-bis-(dicyano-amide)

sodium hydroxide
1310-73-2

sodium hydroxide

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
zinc dicyanamide

zinc dicyanamide

sodium hydroxide
1310-73-2

sodium hydroxide

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
copper(II) dicyanamide
14890-16-5, 18447-47-7, 21962-69-6

copper(II) dicyanamide

sodium carbonate
497-19-8

sodium carbonate

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
dicyanamide; calcium-bis-(dicyano-amide)
14723-18-3

dicyanamide; calcium-bis-(dicyano-amide)

sodium carbonate
497-19-8

sodium carbonate

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
In water
In water
dicyanamide; calcium-bis-(dicyano-amide)
14723-18-3

dicyanamide; calcium-bis-(dicyano-amide)

sodium sulfate
7757-82-6

sodium sulfate

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In water
In water
sodium carbonate
497-19-8

sodium carbonate

zinc dicyanamide

zinc dicyanamide

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
In not given synthesis from dicyanamide suspn. and Na salt soln.; filtration; evapn. under reduced pressure up to crystn.;;
sodium dicyanimide *H2O

sodium dicyanimide *H2O

sodium dicyanamide
1934-75-4

sodium dicyanamide

Conditions
ConditionsYield
In neat (no solvent) byproducts: H2O; at 160°C;;
In neat (no solvent) byproducts: H2O; at 160°C;;
sodium dicyanamide
1934-75-4

sodium dicyanamide

4-chloro-aniline
106-47-8

4-chloro-aniline

1-(4-chlorophenyl)-3-cyanoguanidine
1482-62-8

1-(4-chlorophenyl)-3-cyanoguanidine

Conditions
ConditionsYield
oxonium; acetic acid In water at 40℃; Rate constant; Mechanism;100%
With hydrogenchloride In water at 60℃; for 3h;87%
Stage #1: sodium dicyanamide; 4-chloro-aniline With hydrogenchloride In water at 50 - 90℃; for 18h;
Stage #2: With sodium hydrogencarbonate In water for 0.25h;
78.3%
sodium dicyanamide
1934-75-4

sodium dicyanamide

5-amino-2-methyl-1-(1-ethylpropyl)indole hydrochloride

5-amino-2-methyl-1-(1-ethylpropyl)indole hydrochloride

N-cyano-N'-[2-methyl-1-(1-ethylpropyl)indol-5-yl]guanidine

N-cyano-N'-[2-methyl-1-(1-ethylpropyl)indol-5-yl]guanidine

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 50℃; for 4h;100%
Methyl 3-aminobenzoate
4518-10-9

Methyl 3-aminobenzoate

sodium dicyanamide
1934-75-4

sodium dicyanamide

methyl 3-[amino(cyanoiminomethyl)]aminobenzoate
93070-47-4

methyl 3-[amino(cyanoiminomethyl)]aminobenzoate

Conditions
ConditionsYield
With hydrogenchloride at 80 - 90℃; for 2h;100%
sodium dicyanamide
1934-75-4

sodium dicyanamide

1-n-butyl-3-methylimidazolim bromide
85100-77-2

1-n-butyl-3-methylimidazolim bromide

1-buthyl-3-methylimidazolium dicyanamide
448245-52-1

1-buthyl-3-methylimidazolium dicyanamide

Conditions
ConditionsYield
In acetone at 20℃; for 2h;100%
Stage #1: sodium dicyanamide With silver nitrate
Stage #2: 1-n-butyl-3-methylimidazolim bromide In water
ammonium chloride

ammonium chloride

sodium dicyanamide
1934-75-4

sodium dicyanamide

ammonium dicyanamide

ammonium dicyanamide

Conditions
ConditionsYield
With ion-exchange resin; silver nitrate In water ion exchange of aq. NH4(N(CN)2) with acidic form of ion-exchange resin umtil the pH is 4-5, washing the resin with water, chloride removal with AgNO3, pouring soln. of sodium dicyanamide onto the column; evapn. the eluate at room temp.;100%
In water loading aq. soln. of NH4Cl on a column with ion exchange resin (Merck, Ionenaustauscher I, H(+)-Form, Art. 4765), washing with water, loading with a soln. of sodium salt; evapn. at room temp.;99%
In water ion-exchange column was charged with NH4Cl and NaN(CN)2 soln. was passedthrough; soln. was evapd. at room temp.;
zinc(II) nitrate trihydrate

zinc(II) nitrate trihydrate

sodium dicyanamide
1934-75-4

sodium dicyanamide

zinc dicyanamide

zinc dicyanamide

Conditions
ConditionsYield
In water pptn. on addn. of Zn-salt to 2 equiv. cyanamide (stirring); collection (filtration), drying (vac., over P2O5, 2 h); single crystals from mother liquor;100%
[Cu(bis(2-pyrimidylcarbonyl)amidate)(H2O)3]NO3*2H2O

[Cu(bis(2-pyrimidylcarbonyl)amidate)(H2O)3]NO3*2H2O

water
7732-18-5

water

sodium dicyanamide
1934-75-4

sodium dicyanamide

[Cu(bis(2-pyrimidylcarbonyl)amidate)(dicyanamide)(H2O)]2
1017235-46-9

[Cu(bis(2-pyrimidylcarbonyl)amidate)(dicyanamide)(H2O)]2

Conditions
ConditionsYield
In water equimolar aq. soln. of Cu-compound slowly diffused into aq. Na-compound for 1 month at room temp.; elem. anal.;100%
aniline hydrochloride
142-04-1

aniline hydrochloride

sodium dicyanamide
1934-75-4

sodium dicyanamide

1-phenyl-3-cyanoguanidine
41410-39-3

1-phenyl-3-cyanoguanidine

Conditions
ConditionsYield
In butan-1-ol Reflux;100%
1,2-diaminoethane dihydrochloride
333-18-6

1,2-diaminoethane dihydrochloride

sodium dicyanamide
1934-75-4

sodium dicyanamide

1,2-bis(N3-cyano-N1-guanidino)ethane
7408-98-2

1,2-bis(N3-cyano-N1-guanidino)ethane

Conditions
ConditionsYield
In butan-1-ol for 15h; Reflux;99%
With butan-1-ol
copper(II) nitrate trihydrate

copper(II) nitrate trihydrate

sodium dicyanamide
1934-75-4

sodium dicyanamide

2-(1H-imidazolyl)pyridine
25700-14-5

2-(1H-imidazolyl)pyridine

[Cu(II)(2-(2-pyridyl)imidazole)(H2O)(dicyanamide)]n(NO3)n

[Cu(II)(2-(2-pyridyl)imidazole)(H2O)(dicyanamide)]n(NO3)n

Conditions
ConditionsYield
In water elem. anal.;99%
[2,2]bipyridinyl
366-18-7

[2,2]bipyridinyl

copper(II) nitrate trihydrate

copper(II) nitrate trihydrate

sodium dicyanamide
1934-75-4

sodium dicyanamide

catena-poly[[(2,2'-bipyridine-κ2-N:N')(dicyanamido-κN)copper(II)]-μ-dicyanamido-κ2-N:N']

catena-poly[[(2,2'-bipyridine-κ2-N:N')(dicyanamido-κN)copper(II)]-μ-dicyanamido-κ2-N:N']

Conditions
ConditionsYield
In water elem. anal.;99%
copper(II) nitrate trihydrate

copper(II) nitrate trihydrate

sodium dicyanamide
1934-75-4

sodium dicyanamide

2,2'-Bipyrimidine
34671-83-5

2,2'-Bipyrimidine

[Cu(2,2'-bipyrimidine)(dicyanamide)2]n

[Cu(2,2'-bipyrimidine)(dicyanamide)2]n

Conditions
ConditionsYield
In water elem. anal.;99%
di(pyridin-2-yl)amine
1202-34-2

di(pyridin-2-yl)amine

copper(II) nitrate trihydrate

copper(II) nitrate trihydrate

sodium dicyanamide
1934-75-4

sodium dicyanamide

[Cu(II)(2,2'-dipyridylamine)(dicyanamide)2]n

[Cu(II)(2,2'-dipyridylamine)(dicyanamide)2]n

Conditions
ConditionsYield
In water elem. anal.;99%
diaqua{bis(2-pyridylcarbonyl)-amido}copper(II) nitrate dihydrate
127887-62-1

diaqua{bis(2-pyridylcarbonyl)-amido}copper(II) nitrate dihydrate

sodium dicyanamide
1934-75-4

sodium dicyanamide

[Cu(bis(2-pyridylcarbonyl)amidate)(H2O)(dicyanamide)]2
428509-66-4

[Cu(bis(2-pyridylcarbonyl)amidate)(H2O)(dicyanamide)]2

Conditions
ConditionsYield
In water react. stoich. amts. (Cu(bpca)(H2O)2)NO3*2H2O and sodium dicyanamide; elem. anal.;99%
copper(II) nitrate trihydrate

copper(II) nitrate trihydrate

2.9-dimethyl-1,10-phenanthroline
484-11-7

2.9-dimethyl-1,10-phenanthroline

sodium dicyanamide
1934-75-4

sodium dicyanamide

[Cu2(2,9-dimethyl-1,10-phenanthroline)2(dicyanamide)4]
758716-17-5

[Cu2(2,9-dimethyl-1,10-phenanthroline)2(dicyanamide)4]

Conditions
ConditionsYield
In water addn. of aq. soln. of NaN(CN)2 to aq. soln. of Cu(NO3)2*3H2O and 2,9-dimethyl-1,10-phenanthroline; crystn., elem. anal.;99%
4,4'-dimethyl-2,2'-bipyridines
1134-35-6

4,4'-dimethyl-2,2'-bipyridines

copper(II) nitrate trihydrate

copper(II) nitrate trihydrate

sodium dicyanamide
1934-75-4

sodium dicyanamide

[Cu(4,4'-dimethyl-2,2'-bipyridine)(dicyanamide)2(H2O)]
758716-19-7

[Cu(4,4'-dimethyl-2,2'-bipyridine)(dicyanamide)2(H2O)]

Conditions
ConditionsYield
In water slow diffusion in an H-shaped tube containing aq. soln. Cu(4,4'-dimethyl-2,2'-bipyridine)(NO3)2 (mixt. of Cu(NO3)2*3H2O and 4,4'-dimethyl-2,2'-bipyridine in stoich. amts) in one arm and NaN(CN)2 in the other for 15 days; crystn., elem. anal.;99%
pyridine-3-carbonitrile
100-54-9

pyridine-3-carbonitrile

iron(II) perchlorate hexahydrate

iron(II) perchlorate hexahydrate

sodium dicyanamide
1934-75-4

sodium dicyanamide

[Fe(dicyanamide)2(3-cyanopyridine)2]n

[Fe(dicyanamide)2(3-cyanopyridine)2]n

Conditions
ConditionsYield
In methanol; water; acetonitrile powder X-ray diffraction;99%
In methanol; water; acetonitrile soln. 3-CNpy and Na(N(CN)2) in MeCN-MeOH was heated for 5 min, aq. soln.Fe(ClO4)2*6H2O was added; soln. was filtered and left to stand at room temp. for 3 weeks; elem. anal.;15%
3-methyl-1-(ethoxyethoxycarbonylmethyl)imidazolium bromide
1122146-50-2

3-methyl-1-(ethoxyethoxycarbonylmethyl)imidazolium bromide

sodium dicyanamide
1934-75-4

sodium dicyanamide

3-methyl-1-(ethoxyethoxycarbonylmethyl)imidazolium dicyanoamide
1122146-55-7

3-methyl-1-(ethoxyethoxycarbonylmethyl)imidazolium dicyanoamide

Conditions
ConditionsYield
In acetonitrile for 96h; Reflux;99%
3-methyl-1-(ethoxyethoxyethoxycarbonylmethyl)imidazolium bromide
1122146-78-4

3-methyl-1-(ethoxyethoxyethoxycarbonylmethyl)imidazolium bromide

sodium dicyanamide
1934-75-4

sodium dicyanamide

3-methyl-1-(ethoxyethoxyethoxycarbonylmethyl)imidazolium dicyanoamide
1122146-83-1

3-methyl-1-(ethoxyethoxyethoxycarbonylmethyl)imidazolium dicyanoamide

Conditions
ConditionsYield
In acetonitrile for 96h; Reflux;99%
2,3-dimethyl-1-(methoxyethoxyethoxycarbonylmethyl)imidazolium bromide
1122147-13-0

2,3-dimethyl-1-(methoxyethoxyethoxycarbonylmethyl)imidazolium bromide

sodium dicyanamide
1934-75-4

sodium dicyanamide

2,3-dimethyl-1-(methoxyethoxyethoxycarbonylmethyl)imidazolium dicyanoamide
1122147-18-5

2,3-dimethyl-1-(methoxyethoxyethoxycarbonylmethyl)imidazolium dicyanoamide

Conditions
ConditionsYield
In acetonitrile for 96h; Reflux;99%
1-methyl-3-(11-ethoxycarbonyl-undecyl)imidazolium bromide
1000995-41-4

1-methyl-3-(11-ethoxycarbonyl-undecyl)imidazolium bromide

sodium dicyanamide
1934-75-4

sodium dicyanamide

[C10O2EtMIM][DCA]
1265530-16-2

[C10O2EtMIM][DCA]

Conditions
ConditionsYield
In dichloromethane at 20℃; for 48h;99%
sodium dicyanamide
1934-75-4

sodium dicyanamide

1-(2,4-dinitrophenyl)-pyridinium chloride
4185-69-7

1-(2,4-dinitrophenyl)-pyridinium chloride

C11H8N3O4(1+)*C2N3(1-)

C11H8N3O4(1+)*C2N3(1-)

Conditions
ConditionsYield
In methanol at 20℃; for 18h; Inert atmosphere;99%
sodium dicyanamide
1934-75-4

sodium dicyanamide

silver nitrate

silver nitrate

silver dicyanamide
51342-29-1

silver dicyanamide

Conditions
ConditionsYield
In water at 20℃;98%
In water at 20℃; for 1h; Darkness;97%
In water95%
N-methoxylamine hydrochloride
593-56-6

N-methoxylamine hydrochloride

sodium dicyanamide
1934-75-4

sodium dicyanamide

1-cyano-2-methoxyguanidine
1108717-36-7

1-cyano-2-methoxyguanidine

Conditions
ConditionsYield
In ethanol at 20℃;98%
1-methyl-3-(pentoxycarbonylmethyl)imidazolium bromide
808184-34-1

1-methyl-3-(pentoxycarbonylmethyl)imidazolium bromide

sodium dicyanamide
1934-75-4

sodium dicyanamide

3-methyl-1-(pentoxycarbonylmethyl)imidazolium dicyanoamide

3-methyl-1-(pentoxycarbonylmethyl)imidazolium dicyanoamide

Conditions
ConditionsYield
In acetonitrile for 96h; Reflux;98%
3-{2-[2-(2-butoxyethoxy)ethoxy]-2-oxoethyl}-1-methyl-1H-imidazol-3-ium bromide
1122146-92-2

3-{2-[2-(2-butoxyethoxy)ethoxy]-2-oxoethyl}-1-methyl-1H-imidazol-3-ium bromide

sodium dicyanamide
1934-75-4

sodium dicyanamide

3-methyl-1-(butoxyethoxyethoxycarbonylmethyl)imidazolium dicyanoamide
1122146-97-7

3-methyl-1-(butoxyethoxyethoxycarbonylmethyl)imidazolium dicyanoamide

Conditions
ConditionsYield
In acetonitrile for 96h; Reflux;98%
1-(3-phenoxypropyl)-4-((2-(1-(3-phenoxypropyl)pyridin-1-ium-4‑carbonyl)hydrazono)methyl)pyridin-1-ium bromide

1-(3-phenoxypropyl)-4-((2-(1-(3-phenoxypropyl)pyridin-1-ium-4‑carbonyl)hydrazono)methyl)pyridin-1-ium bromide

sodium dicyanamide
1934-75-4

sodium dicyanamide

1-(3-phenoxypropyl)-4-((2-(1-(3-phenoxypropyl)pyridin-1-ium-4‑carbonyl)hydrazono)methyl)pyridin-1-ium dicyanamide

1-(3-phenoxypropyl)-4-((2-(1-(3-phenoxypropyl)pyridin-1-ium-4‑carbonyl)hydrazono)methyl)pyridin-1-ium dicyanamide

Conditions
ConditionsYield
In acetonitrile for 0.166667h; Microwave irradiation;98%
1-(4-phenoxybutyl)-3-((2-(1-(4-phenoxybutyl)pyridin-1-ium-4‑carbonyl)hydrazono)methyl)pyridin-1-ium bromide

1-(4-phenoxybutyl)-3-((2-(1-(4-phenoxybutyl)pyridin-1-ium-4‑carbonyl)hydrazono)methyl)pyridin-1-ium bromide

sodium dicyanamide
1934-75-4

sodium dicyanamide

1-(4-phenoxybutyl)-3-((2-(1-(4-phenoxybutyl)pyridin-1-ium-4‑carbonyl)hydrazono)methyl)pyridin-1-ium dicyanamide

1-(4-phenoxybutyl)-3-((2-(1-(4-phenoxybutyl)pyridin-1-ium-4‑carbonyl)hydrazono)methyl)pyridin-1-ium dicyanamide

Conditions
ConditionsYield
In acetonitrile for 0.166667h; Microwave irradiation;98%
1‐(2‐methoxyphenyl)‐3‐octyl‐imidazolium bromide

1‐(2‐methoxyphenyl)‐3‐octyl‐imidazolium bromide

sodium dicyanamide
1934-75-4

sodium dicyanamide

1‐(2‐methoxyphenyl)‐3‐octyl‐imidazolium dicyanamide

1‐(2‐methoxyphenyl)‐3‐octyl‐imidazolium dicyanamide

Conditions
ConditionsYield
In water at 20℃; for 48h;98%
3,9-bis(3-aminopropyl)-2,4,8,10-tetraoxaspiro[5.5]undecane dihydrochloride

3,9-bis(3-aminopropyl)-2,4,8,10-tetraoxaspiro[5.5]undecane dihydrochloride

sodium dicyanamide
1934-75-4

sodium dicyanamide

butan-1-ol
71-36-3

butan-1-ol

3,9-bis(3-cyanoguanidinopropyl)-2,4,8,10-tetraoxaspiro[5.5]undecane

3,9-bis(3-cyanoguanidinopropyl)-2,4,8,10-tetraoxaspiro[5.5]undecane

Conditions
ConditionsYield
97.5%

1934-75-4Relevant articles and documents

Synthesis, characterization and structure of metallocene dicyanamide complexes

Honzí?ek, Jan,Erben, Milan,Císa?ová, Ivana,Vinklárek, Jaromír

, p. 814 - 819 (2005)

The bis(cyclopentadienyl) complexes [Cp2Ti(dca)]2O and Cp2V(dca)2 (dca = dicyanamide) have been prepared by reaction of sodium dicyanamide with aqueous solution of titanocene dichloride and vanadocene dichloride

Method of producing sodium dicyanamide

-

Page/Page column 6, (2008/06/13)

A process is described for preparing sodium dicyanamide, in which cyanamide is reacted simultaneously with sodium hydroxide solution and cyanogen chloride in aqueous solution at temperatures of 20 to 100° and a pH of 7.0 to 10.0. By means of the inventive process it is possible, starting from raw materials which are available in technical-grade quality, to prepare sodium dicyanamide in good yields of 75 to 95% and very high purities of up to 100% in a very environmentally friendly manner, for which reason this process is particularly highly suitable for the industrial scale.

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