3,6-bis[2-(2-{2-[2-(toluene-4-sulphonyl)ethoxy]ethoxy}ethoxy)ethoxy]phthalonitrile

Base Information

Chemical Name:3,6-bis[2-(2-{2-[2-(toluene-4-sulphonyl)ethoxy]ethoxy}ethoxy)ethoxy]phthalonitrile
CAS No.:1480891-02-8
Molecular Formula:C₃₈H₄₈N₂O₁₄S₂
Molecular Weight:820.936
Hs Code.:

Synonyms:3,6-bis[2-(2-{2-[2-(toluene-4-sulphonyl)ethoxy]ethoxy}ethoxy)ethoxy]phthalonitrile

Suppliers and Price of 3,6-bis[2-(2-{2-[2-(toluene-4-sulphonyl)ethoxy]ethoxy}ethoxy)ethoxy]phthalonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,6-bis[2-(2-{2-[2-(toluene-4-sulphonyl)ethoxy]ethoxy}ethoxy)ethoxy]phthalonitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,6-bis[2-(2-{2-[2-(toluene-4-sulphonyl)ethoxy]ethoxy}ethoxy)ethoxy]phthalonitrile

There total 2 articles about 3,6-bis[2-(2-{2-[2-(toluene-4-sulphonyl)ethoxy]ethoxy}ethoxy)ethoxy]phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 37860-51-8
tetraethylene glycol di(p-toluenesulfonate)

: 4733-50-0
2,3-dicyano-1,4-hydroquinone

: 1480891-02-8
3,6-bis[2-(2-{2-[2-(toluene-4-sulphonyl)ethoxy]ethoxy}ethoxy)ethoxy]phthalonitrile

Guidance literature:: In acetonitrile; at 60 ℃; for 240h; Inert atmosphere; Schlenk technique;
DOI:10.1142/S1088424613500594

Reference yield: 36.0%

: 4733-50-0
2,3-dicyano-1,4-hydroquinone

: 77544-60-6
p-toluenesulfonic acid 2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethyl ester

: 1480891-02-8
3,6-bis[2-(2-{2-[2-(toluene-4-sulphonyl)ethoxy]ethoxy}ethoxy)ethoxy]phthalonitrile

Guidance literature:: 2,3-dicyano-1,4-hydroquinone; p-toluenesulfonic acid 2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethyl ester; With sodium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; at 80 ℃;

With p-toluenesulfonyl chloride; potassium hydroxide; at 20 ℃; for 5h;

Reference yield: 51.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1480891-02-8
3,6-bis[2-(2-{2-[2-(toluene-4-sulphonyl)ethoxy]ethoxy}ethoxy)ethoxy]phthalonitrile

: 121492-06-6
(2-aminoethyl)methylcarbamic acid tert-butyl ester

: C₅₀H₈₄N₆O₁₆

Guidance literature:: 3,6-bis[2-(2-{2-[2-(toluene-4-sulphonyl)ethoxy]ethoxy}ethoxy)ethoxy]phthalonitrile; (2-aminoethyl)methylcarbamic acid tert-butyl ester; In 1,4-dioxane; at 70 ℃;

di-tert-butyl dicarbonate; In 1,4-dioxane; at 20 ℃; for 12h;