-N-<(R)-α-methylbenzyl>amino>acetonitrile

Base Information

Chemical Name:-N-<(R)-α-methylbenzyl>amino>acetonitrile
CAS No.:98237-97-9
Molecular Formula:C₁₅H₂₀N₂O
Molecular Weight:244.337
Hs Code.:

<N-<(1R,2R)-2-hydroxycyclopentyl>-N-<(R)-α-methylbenzyl>amino>acetonitrile

Synonyms:-N-<(R)-α-methylbenzyl>amino>acetonitrile

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Chemical Property of -N-<(R)-α-methylbenzyl>amino>acetonitrile

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Technology Process of -N-<(R)-α-methylbenzyl>amino>acetonitrile

There total 1 articles about -N-<(R)-α-methylbenzyl>amino>acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 151-50-8
potassium cyanide

: (1R,2R)-2-((R)-1-Phenyl-ethylamino)-cyclopentanol; hydrochloride

: 98237-97-9
-N-<(R)-α-methylbenzyl>amino>acetonitrile

Guidance literature:: for 10h; Ambient temperature;
DOI:10.1002/hlca.19850680324

Reference yield: 95.0%

: 98237-97-9
-N-<(R)-α-methylbenzyl>amino>acetonitrile

: 98244-61-2
-N-<(1R)-2-oxocyclopentyl>amino>acetonitrile

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; for 10h; Ambient temperature;
DOI:10.1002/hlca.19850680324

Reference yield:

: 98237-97-9
-N-<(R)-α-methylbenzyl>amino>acetonitrile

: 3-Benzo[1,3]dioxol-5-yl-1-[[(1R,2R)-2-(1-benzo[1,3]dioxol-5-yl-vinyl)-2-hydroxy-cyclopentyl]-((R)-1-phenyl-ethyl)-amino]-but-3-en-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / oxalyl chloride, DMSO / CH₂Cl₂ / 10 h / Ambient temperature

2: tetrahydrofuran / -60 °C

With oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/hlca.19850680324