methyl (2S)-{[(2-amino-4-fluorophenyl)carbonyl]amino}(cyclohexyl)-ethanoate

Base Information

• Chemical Name: methyl (2S)-{[(2-amino-4-fluorophenyl)carbonyl]amino}(cyclohexyl)-ethanoate
• CAS No.: 887243-09-6
• Molecular Formula: C₁₆H₂₁FN₂O₃
• Molecular Weight: 308.353

Synonyms:methyl (2S)-{[(2-amino-4-fluorophenyl)carbonyl]amino}(cyclohexyl)-ethanoate

Chemical Property of methyl (2S)-{[(2-amino-4-fluorophenyl)carbonyl]amino}(cyclohexyl)-ethanoate

Chemical Property:

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Technology Process of methyl (2S)-{[(2-amino-4-fluorophenyl)carbonyl]amino}(cyclohexyl)-ethanoate

There total 1 articles about methyl (2S)-{[(2-amino-4-fluorophenyl)carbonyl]amino}(cyclohexyl)-ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

methyl (2S)-cyclohexyl-{[(4-fluoro-2-nitrophenyl)carbonyl]amino}ethanoate (887243-08-5) → methyl (2S)-{[(2-amino-4-fluorophenyl)carbonyl]amino}(cyclohexyl)-ethanoate (887243-09-6)

Guidance literature:

With hydrogen; 5% palladium over charcoal; In ethanol; for 1h; under 2585.81 Torr;

Reference yield: 86.0%

methyl (2S)-{[(2-amino-4-fluorophenyl)carbonyl]amino}(cyclohexyl)-ethanoate (887243-09-6) + 1,3-dichloro-2-isocyanato-5-[(trifluoromethyl)oxy]benzene → methyl (2S)-cyclohexyl-{[(2-{[({2,6-dichloro-4-[(trifluoromethyl)oxy]phenyl}amino)carbonyl]amino}-4-fluorophenyl)carbonyl]amino}ethanoate (887243-39-2)

Guidance literature:

With pyridine; at 20 ℃;

Reference yield: 71.0%

methyl (2S)-{[(2-amino-4-fluorophenyl)carbonyl]amino}(cyclohexyl)-ethanoate (887243-09-6) + 2,6-dimethylphenylisocyanate (28556-81-2) → methyl (2S)-cyclohexyl-({[2-({[(2,6-dimethylphenyl)amino]carbonyl}-amino)-4-fluorophenyl]carbonyl}amino)ethanoate (887243-10-9)

Guidance literature:

With pyridine; at 20 ℃;

upstream raw materials:

methyl (2S)-cyclohexyl-{[(4-fluoro-2-nitrophenyl)carbonyl]amino}ethanoate

Downstream raw materials:

methyl (2S)-cyclohexyl-({[2-({[(2,6-dimethylphenyl)amino]carbonyl}-amino)-4-fluorophenyl]carbonyl}amino)ethanoate

methyl (2S)-cyclohexyl-{[(2-{[({2,6-dichloro-4-[(trifluoromethyl)oxy]phenyl}amino)carbonyl]amino}-4-fluorophenyl)carbonyl]amino}ethanoate

C₂₅H₂₉BrFN₃O₄

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