Carbamic acid, [(2,2-dimethylhydrazino)carbonyl]methyl-, methyl ester (9CI)

Base Information

• Chemical Name: Carbamic acid, [(2,2-dimethylhydrazino)carbonyl]methyl-, methyl ester (9CI)
• CAS No.: 103836-50-6
• Molecular Formula: C6H13 N3 O3
• Molecular Weight: 175.188
• Mol file: 103836-50-6.mol

Synonyms:Carbamic acid, [(2,2-dimethylhydrazino)carbonyl]methyl-, methyl ester (9CI)

Chemical Property of Carbamic acid, [(2,2-dimethylhydrazino)carbonyl]methyl-, methyl ester (9CI)

Chemical Property:

• PSA: 61.88000
• LogP: 0.26170

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [(2,2-dimethylhydrazino)carbonyl]methyl-, methyl ester (9CI)

There total 2 articles about Carbamic acid, [(2,2-dimethylhydrazino)carbonyl]methyl-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,4-trimethyl-1,2,4-triazolidine-3,5-dione 1,2-ylide (54133-08-3) → methyl N-methylcarbamate (6642-30-4) + 1,1,4-trimethyl-4-(methoxycarbonyl)semicarbazide (103836-50-6) + N,N-dimethyl-N'-carbomethoxyhydrazine (55741-07-6)

Guidance literature:

With methanol; In dichloromethane; for 42.7h; Irradiation;

DOI:10.1021/jo00370a020

Reference yield:

methanol (67-56-1) + 1,1,4-trimethyl-1,2,4-triazolidine-3,5-dione 1,2-ylide (54133-08-3) → methyl N-methylcarbamate (6642-30-4) + 1,1,4-trimethyl-4-(methoxycarbonyl)semicarbazide (103836-50-6) + N,N-dimethyl-N'-carbomethoxyhydrazine (55741-07-6)

Guidance literature:

In dichloromethane; for 42.7h; Irradiation;

DOI:10.1021/jo00370a020

upstream raw materials:

methanol

1,1,4-trimethyl-1,2,4-triazolidine-3,5-dione 1,2-ylide