methyl 11-(1-methyl-4-piperidinyl)-11H-dibenzo[b,e][1,4]oxathiepin-2-yl ether

Base Information

Chemical Name:methyl 11-(1-methyl-4-piperidinyl)-11H-dibenzo[b,e][1,4]oxathiepin-2-yl ether
CAS No.:83975-95-5
Molecular Formula:C₂₀H₂₃NO₂S
Molecular Weight:341.474
Hs Code.:
Mol file:83975-95-5.mol

Synonyms:8-Methoxy-6-(1-methyl-4-piperidyl)-6H-dibenz-1,4-oxathiepin

Suppliers and Price of methyl 11-(1-methyl-4-piperidinyl)-11H-dibenzo[b,e][1,4]oxathiepin-2-yl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 11-(1-methyl-4-piperidinyl)-11H-dibenzo[b,e][1,4]oxathiepin-2-yl ether

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Technology Process of methyl 11-(1-methyl-4-piperidinyl)-11H-dibenzo[b,e][1,4]oxathiepin-2-yl ether

There total 5 articles about methyl 11-(1-methyl-4-piperidinyl)-11H-dibenzo[b,e][1,4]oxathiepin-2-yl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 83986-15-6
[2-(2-Fluoro-phenylsulfanyl)-5-methoxy-phenyl]-(1-methyl-piperidin-4-yl)-methanol

: 40478-82-8
2-methoxy-9H-thioxanthen-9-one

: 83975-95-5
8-Methoxy-6-(1-methyl-4-piperidyl)-6H-dibenz-1,4-oxathiepin

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 70 ℃; for 11h;
DOI:10.1135/cccc19823077

Reference yield:

: 2557-78-0
2-fluorothiophenol

: 83975-95-5
8-Methoxy-6-(1-methyl-4-piperidyl)-6H-dibenz-1,4-oxathiepin

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / K₂CO₃ / Cu / dimethylformamide / 6 h / 150 °C

2: 1) Mg / 1) THF; 2) THF, reflux, 4 h

3: 76 percent / NaH / dimethylformamide / 11 h / 70 °C

With sodium hydride; potassium carbonate; magnesium; copper; In N,N-dimethyl-formamide;
DOI:10.1135/cccc19823077

Reference yield:

: 7507-86-0
2-bromo-5-methoxy-benzaldehyde

: 83975-95-5
8-Methoxy-6-(1-methyl-4-piperidyl)-6H-dibenz-1,4-oxathiepin

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / K₂CO₃ / Cu / dimethylformamide / 6 h / 150 °C

2: 1) Mg / 1) THF; 2) THF, reflux, 4 h

3: 76 percent / NaH / dimethylformamide / 11 h / 70 °C

With sodium hydride; potassium carbonate; magnesium; copper; In N,N-dimethyl-formamide;
DOI:10.1135/cccc19823077