Technology Process of C36H55N5O5S
There total 22 articles about C36H55N5O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium cyanoborohydride;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: hydrogenchloride / 1,4-dioxane / 0 °C
2.1: 2-bromo-1-ethylpyridin-1-ium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / -10 - 20 °C
3.1: hydrogen bromide / acetic acid / 0 °C
4.1: sodium hydrogencarbonate / water
4.2: -20 - 20 °C
5.1: sodium hydroxide / 1,4-dioxane / 0 °C
5.2: pH 2
6.1: 4-methyl-morpholine / tetrahydrofuran / 0.17 h
7.1: 4-methyl-morpholine / tetrahydrofuran / -20 - 20 °C
8.1: hydrogen bromide / acetic acid / 0 °C
9.1: methanol / 3 h / 20 °C
With
4-methyl-morpholine; hydrogenchloride; hydrogen bromide; 2-bromo-1-ethylpyridin-1-ium tetrafluoroborate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetic acid;
DOI:10.1002/ejoc.200900999
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: hydrogen bromide / acetic acid / 0 °C
2.1: sodium hydrogencarbonate / water
2.2: -20 - 20 °C
3.1: sodium hydroxide / 1,4-dioxane / 0 °C
3.2: pH 2
4.1: 4-methyl-morpholine / tetrahydrofuran / 0.17 h
5.1: 4-methyl-morpholine / tetrahydrofuran / -20 - 20 °C
6.1: hydrogen bromide / acetic acid / 0 °C
7.1: methanol / 3 h / 20 °C
With
4-methyl-morpholine; hydrogen bromide; sodium hydrogencarbonate; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; water; acetic acid;
DOI:10.1002/ejoc.200900999
