Technology Process of C61H80N4O16S2
There total 7 articles about C61H80N4O16S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C59H76N4O16S2;
With
sodium hydride;
In
tetrahydrofuran;
for 0.166667h;
methyl iodide;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1002/chem.201000611
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / dichloromethane / 20 °C
2.1: sodium hydride / tetrahydrofuran / 0.17 h
2.2: 20 °C
With
sodium hydride; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201000611
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium azide / ethanol / 8 h / Reflux
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h
3.2: 20 °C
4.1: triphenylphosphine / tetrahydrofuran / 8 h / 20 °C
4.2: 48 h
5.1: triethylamine / dichloromethane / 20 °C
6.1: sodium hydride / tetrahydrofuran / 0.17 h
6.2: 20 °C
With
sodium azide; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
3.1: Williamson reaction / 3.2: Williamson reaction / 4.1: Staudinger reaction / 4.2: Staudinger reaction;
DOI:10.1002/chem.201000611