(R)-3-methyl-4-(phenylsulfonyl)butan-1-ol tert-butyldimethylsilyl ether

Base Information

Chemical Name:(R)-3-methyl-4-(phenylsulfonyl)butan-1-ol tert-butyldimethylsilyl ether
CAS No.:1331743-67-9
Molecular Formula:C₁₇H₃₀O₃SSi
Molecular Weight:342.575
Hs Code.:

Synonyms:(R)-3-methyl-4-(phenylsulfonyl)butan-1-ol tert-butyldimethylsilyl ether

Suppliers and Price of (R)-3-methyl-4-(phenylsulfonyl)butan-1-ol tert-butyldimethylsilyl ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (R)-3-methyl-4-(phenylsulfonyl)butan-1-ol tert-butyldimethylsilyl ether

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of (R)-3-methyl-4-(phenylsulfonyl)butan-1-ol tert-butyldimethylsilyl ether

There total 4 articles about (R)-3-methyl-4-(phenylsulfonyl)butan-1-ol tert-butyldimethylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1331743-65-7
(R)-3-methyl-4,4-bis(phenylsulfonyl)butan-1-ol tert-butyldimethylsilyl ether

: 1331743-67-9
(R)-3-methyl-4-(phenylsulfonyl)butan-1-ol tert-butyldimethylsilyl ether

Guidance literature:: With samarium diiodide; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c1cc13232f

Reference yield:

: 1201829-81-3
(R)-3-methyl-4,4-bis(phenylsulfonyl)butanal

: 1331743-67-9
(R)-3-methyl-4-(phenylsulfonyl)butan-1-ol tert-butyldimethylsilyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 2 h / 0 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C

3: samarium diiodide / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; samarium diiodide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1039/c1cc13232f

Reference yield:

: 1186231-90-2
(R)-3-methyl-4,4-bis(phenylsulfonyl)butan-1-ol

: 1331743-67-9
(R)-3-methyl-4-(phenylsulfonyl)butan-1-ol tert-butyldimethylsilyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C

2: samarium diiodide / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With 1H-imidazole; samarium diiodide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c1cc13232f